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110 2nd Avenue South,#D7, Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> hg1Lwww mccampbell corn E-mail main@mccampbell com <br /> Advanced GeoEnvironmental Client Project ID Flag City Date Sampled 06/13/02 <br /> 837 Shaw Road Date Received 06/14/02 <br /> Stockton,CA 95215 Client Contact Tim Cuellar Date Extracted 06/14/02 <br /> [Client P O [Date Analyzed 06/14-06/17/02 <br /> Metals' <br /> EPA methods 6010/200 7 7470n4711245 11241LHH ,7060/206 2 As) 7740/270 2(Se),7841/279 2 ),239 2 b,w 204 2 Sb,w <br /> Lab ID 0206240-029 <br /> Reporting Limit <br /> Client ID Effluent <br /> Matrix W S W STLC, <br /> TCLP <br /> Extraction' Dissolved TTLC Dissolved <br /> Compound Concentration* mg/kg mg/L mglL <br /> Antimony(Sb) ND 25 00006 005 <br /> Arsenic(As) 00060 25 00005 025 <br /> Banum(Ba) oil 25 0 005 005 <br /> Beryllium(Be) ND 05 00004 001 <br /> • Cadmium(Cd) -- 05 00005 001 <br /> Chromium(Cr) ND 05 0 002 005 <br /> Cobalt(Co) ND 20 0 005 005 <br /> Copper(Cu) ND 20 0 005 005 <br /> Lead(Pb) 000069 30 00005 02 <br /> Molybdenum(Mo) ND 25 0 005 005 <br /> Nickel(Ni) ND 20 0 005 005 <br /> Selenium(Se) ND 25 00005 025 <br /> Silver(Ag) ND 10 0 001 005 <br /> Thallium(Ti) ND 25 00005 05 <br /> Vanadium(V) 0 039 20 0 005 005 <br /> Zinc(Zn) 0011 10 0 005 005 <br /> %Recovery Surrogate NIA <br /> Comments <br /> *water samples are reported in mg/L,sod and sludge samples in mgtkp_wipes in ug/wipe and all TCLP/STLC/SPLP extracts in mg/L <br /> ND means not detected above the reporting limit,NIA means surrogate not applicable to this analysis <br /> °EPA extraction methods 1311(TCLP),3010/3020(water,TrLC),3040(organic matrices TTLC),3050(solids TTLC),STLC-CA Title 22 <br /> DISTLC extractions are performed using STLC methodology except that deioni=d water is substituted for citric acid buffer as the <br /> extraction fluid DISTLC results are not applicable to STLC regulatory limits <br /> • 'surrogate diluted out of range <br /> a reporting limit raised due to matrix interference <br /> i) liquid sample that contains greater than —2 vol % sediment, this sediment is extracted with the liquid, in accordance with EPA <br /> methodola es and can si ificant! effect re orted metal concentrations <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />