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110 2nd Avenue South,#i)7,Pacheco,CA 94553-5560 <br /> McCampbell Analytical, Inc. Telephone 925-798-1620 Fax 925-798-1622 <br /> Website www mccampbell com E-mail mam®mccampbcll cam <br /> Advanced GeoEnvironmental, Inc Client Project ID Flag City Chevron Date Sampled 05/13/04 <br /> 837 SbaW Road Date Received 05/14/04 <br /> Client Contact Tun Cuellar Date Extracted 05/14/04 <br /> Stockton,CA 95215 <br /> Client P O Date Analyzed 05/19/04 <br /> Lead by Graphite Furnace Atom>Ic Absorption* <br /> tracuon method. E200 9 Analytical tneiho& E200 9 <br /> Work Order 0405225 <br /> Lab ID Client 11) Matrix Extraction Lead DF %SS <br /> 0405225-MID Influent W TTLC ND I NIA <br /> h <br /> G <br /> Reporting Limit for DF w1, V1T TTLC 0 005 mgJL <br /> ND means not detected at or <br /> above the reporting limit S TTLC NA mg/kg <br /> *water/producdotUnon-aqueous liquid samples and all TCLP 1 STLC I DISTLC I SPLP extracts arc reported to mg(L.,soil/sludge/solid samples to mg/kg, <br /> wipe samples inµg/wipe filter samples in jig/filter <br /> #means surrogate recovery outside of acceptance range due to matrix interference,&means surrogate diluted out of acceptance range,ND means not <br /> detected above the reporting limit,N/A means not applicable to this sample or instrument. <br /> Analytical Methods EPA 6010C/200 7 for all elements except 200 9(water/liquid-Sb,As,Pb,Se,TI),245 1 (Hg),7010 <br /> (sludge/soilisolid/oil/product/wipe/filier-As,Se,Tl),7471B(Hg) <br /> i)liquid sample that contains greater than--i vol %sediment,this sediment is extracted with the liquid,in accordance with EPA methodologies and can <br /> significantly effect reported metal concentrations,j)reporting limit raised due to insufficient sample amount,k)results are reported by dry weight,y) <br /> estimated values due to low surrogate recovery,z)reporhng limit raised due to matrix interference <br /> • <br /> DHS Certification No 1644J2__Angela Rydehus,Lab Manager <br />