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GeoAnalytical Laboratories, Inc. <br /> 1405 Kansas Avenue Modesto,CA 95351 Phone (209)572-0900 Fax (209)5722-0916 <br /> CERTIFICATE OF ANALYSIS <br /> Wort# Q167-15 Date 7/14/04 <br /> Advanced GeoEnvironmental Date Rec'd 6/15/04 <br /> 837 Shaw Rd Somme Date Started 6/16/04 <br /> Stockton CA 95215 Date Completed 6/20/04 <br /> Project Flag City Chevron Date Sampled 6/15/04 <br /> Time <br /> Sampler <br /> Sample ID Replicate <br /> Lab ID- Q304097 <br /> Aquatic Toxicity <br /> Test Type 96hr static acute % Control 625% 25% 50% 75% 100% <br /> Dilution Water Reconstituted Dl Water Initial pH 7 8 78 7 9 7 8 78 7 8 <br /> Species Pimephales Promelas (Larval) 6/16/04 D O 8 6 8 6 8 7 8 7 8 8 8 8 <br /> Common Name Fathead Minnow Temp°C 194 19 4 195 194 194 194 <br /> Supplier Aqua Tax <br /> Dilution Volume 2,000 ml 24 Hrs pH 78 7 7 7 6 7 6 7 5 75 <br /> #Fish per Dilution 20 6/17/04 DO 8 4 83 84 83 85 82 <br /> Dead in Acclimation rank Temp°C 203 202 203 20 3 203 203 <br /> Age Length Mortalities 0 0 0 0 0 0 <br /> ge Weight 48 H rs pH 78 78 77 7 6 7 5 7 6 <br /> 6118/04 DO 80 82 84 79 81 81 <br /> Temp°C 204 20 4 205 205 204 205 <br /> Mortalities 0 0 0 0 0 0 <br /> Initial Control Hardness 89 72 Ht's pH 7 6 76 77 76 75 7 6 <br /> Final Control Hardness 89 6/19104 D O 8 4 7 6 8 0 77 7 8 7 6 <br /> Temp°C 20 7 20 7 20 6 20 7 207 208 <br /> Mortalities 0 0 0 0 0 0 <br /> 96 Firs. pH 76 75 76 75 75 75 <br /> 6/20/04 DO 78 79 77 76 79 77 <br /> Temp°C 203 20 4 20 3 203 204 201 <br /> Mortalities 0 0 0 0 0 0 <br /> Total Mortalities 0 0 0 0 0 0 <br /> Notes <br /> v <br /> Kanti Gandhi Donna Keller <br /> Chemist Certification # 1157 Laboratory Director <br />