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110 2nd Avenue South,YD7 Pacheco CA 94553 5560 <br /> McCampbell Analytical, fnc. Telephone 925 798-1620 Fax 925-798-1622 <br /> 4 Website www tuccanipbell com E-mail niautQmccampbell.com <br /> . Advanced GeoEnvironmental, Inc Client Project ID Flag City Chevron Date Sampled 06/15/04 <br /> 837 Shaw Road Date Received 06/16/04 <br /> Stockton, CA 95215 Client Contact Tarn Cuellar Date Extracted 06/16/04-06/17/04 <br /> Client P 4 Date Analyzed 06/16/04-06/17104 <br /> Oxygenated Volatile Organacs+EDB and 1,2-DCA by P&7 and GCIMS* <br /> atractwn Method.SW5030B Analytical Method SW8260B Work Order 0406263 <br /> Lab ID 0406263-OIOC 0406263-011C <br /> a <br /> Client ID Influent Effluent <br /> I Reporting Limit for <br /> Matrix W W DF=1 <br /> DF <br /> Compound Concentration ug/kg µg/L <br /> tert-Amyl methyl ether(TAME) ND ND I NA 05 <br /> t-Butyl alcohol(TBA) ND ND NA 50 <br /> 1,2-Dibromoethane(EDB) ND ND <br /> NA OS <br /> 1,2-Dichloroethane(1,2-DCA) ND ND NA 05 <br /> • 011'soprupyl ether(DIPS) ND ND <br /> NA OS <br /> Ethanol ND ! ND NA 50 <br /> Ethyl tent-butyl ether(ETBE) ND f ND NA 0 S <br /> Methanol ND ND NA 500 <br /> Methyl-t-butyl ether(MTBE) 15 ND NA 05 <br /> Surrogate Recoveries(%) <br /> %SS 896 879 <br /> Comments <br /> 'water and vapor samples and all TCLP&SPLP extracts are reported in}ig/L,soil/sludge/solid samples in}ig/kg, wipe samples inµg/wtpe, <br /> product/oil/non-aqueous liquid samples in mglL <br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> #surrogate diluted out of range or surrogate coelutes with another peak <br /> h)lighter than water immiscible sheen/product is present,i)liquid sample that contains gnater than—1 vol %sediment, )sample diluted due to high <br /> Organic content <br /> DHS Certification No 1644 Angela Rydehus, Lab Manager <br />