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110 2nd Avenue South,#D7 Pacheco,CA 94553-5560 <br /> HW:Campbell:Analytical Inc Telephone 925-798-1620 Fax 925-798-1622 <br /> httpd/www nicca=beJLcozn E macs rnaTaTccaumbell coin <br /> (• Advanced GeoEnvironmental,Inc Client Project ID 3 B's Truck Plaza Date Sanipled 06/25/03 <br /> 837 Shaw Road Date Received 06/26/03 <br /> Stockton,CA 95215 Client Contact Tim Cuellar Date Extracted 06/30/03-07102/03 <br /> --rClient P O Date Analyzed 06/30/03-07102/03 <br /> Oxygenates and BTEX by GC/MS* <br /> Extraction Method SW5030H Analytical Method.SW826013 Work Order 9306567 <br /> Lab ID 0306567-OOIB 0306567-002B 0306567-003B 0306567-004B <br /> Client IDDW-1 MWl MW2 MW3 <br /> Reporting Limit for <br /> Matrix W W W W DF=1 <br /> DF 1 33 ; 40 3 100 S W <br /> Compound Concentration ug/kg µg/L <br /> tert-Amyl methyl ether(TAME) ND ND<17 ND<20 ND<50 NA 05 <br /> IBenzene ND 970 1400 2800 NA 0 5 <br /> t-Butyl alcohol(TBA) ND ND<170 ND<200 ND<500 NA 5 0 <br /> 1 2-Dibromoethane(EDS) ND ND<17 ND<20 77 NA 0 5 <br /> 1,2-Dichloroethane(1,2-DCA) ND ND<17 ND<20 ND<50 NA 0 5 <br /> Dusop Wyl ether(DIPS) ND ND<17 ND<20 TTD<50 NA 0 5 <br /> Ethylbenzerie ND 52 130 460 NA 0 5 <br /> Ethyl tert-butyl ether(ETRE) ND ND<17 ND<20 ND<50 NA 0 5 <br /> Methyl-t-butyl ether(MTBE) ND ND<17 23 ND<50 NA 05 <br /> Toluene ND 38 78 470 NA 0 5 <br /> Xylenes ND 130 180 1400 NA 0 5 <br /> Surrogate Recoveries{%} <br /> PSS1 102 105 120 101 <br /> %SS2 95 6 960 969 972 <br /> %SS3 108 101 899 961 <br /> 1 Comments <br /> I *water and vapor samples and all TCLP 8c SPLP extracts are reported inµg/L,soil/sludge/solid samples inµg/kg, wipe samples in jig/wipe, <br /> producr/oil/non-aqueous hgmd samples m mall.. <br /> IND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> #surrogate diluted out of range or surrogate coelutes with another peak. <br /> h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than—2 vol %sediment,j)sample diluted due to high <br /> • organic content <br /> DHS Certification No 1644 Angela Rydelius,Lab Manager <br /> l <br />