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110 2nd Avenue South #D7 Pacheco,CA 94553 5560 <br /> McCampbell Analytical Inc Telephone 925-798-1620 Fax 925-798-1622 <br />' <br /> httpJ/www mccampbcll corn E-mail mam a inccampbell com <br /> • Advanced GeoEnvlronniental, Inc Client Project ID Flag City Chevron Date Sampled 06/27/03 <br />' 837 Shaw Road Date Received 07/01/03 <br /> Stockton, CA 95215 Client Contact Tern Cuellar Date Extracted 07/04/03-07/08/03 <br /> Client P O Date Analyzed 07/04/03-07/08/03 <br /> Oxygenates and BTEX by GC/MS* <br /> Extraction Method SW5030B Analytical Method SW8260B Work Order 0307008 <br />' Lab ID 0307008-OOIB 0307008-002B 0307008-003B 0307008-004B <br /> Client ID MW8B MW8A MW9C MW9B <br /> Reporting Limit for <br />' Matrix W - W – W W DF=1 <br /> DF i 10- —-�� _�---- 1---- <br /> S W <br />' Compound Concentration ug/kg µglL <br /> tert-Amyl methyl ether(TAME) ND ND<5 0 ND ND NA 05 <br />' Benzene ND ND<5 0 ND ND NA 05 <br /> t-Butyl alcohol(TBA) ND ND<50 ND ND NA 50 <br /> Dtisopropyl ether(DQ'E) ND ND<5 0 ND ND NA 05 <br /> Ethanol ND ND<500 ND ND NA 50 <br />'. Ethylbenzene ND ND<5 0 ND ND NA 05 <br /> Ethyl tert-butyl ether(ETBE) ND ND<5 0 ND ND NA 05 <br /> Methanol ND ND<5000 ND ND NA 500 <br /> Methyl-t-butyl ether(MTBE) ND 290 ND ND NA 05 <br /> Toluene ND ND<5 0 ND ND NA 05 <br />' Xylenes 1 7 ND<5 0 ND ND NA 05 <br /> Surrogate Recoveries(%) <br /> 105 106 113 107 <br /> %SS2 990 998 100 976 <br />' %SS3 974 990 103 975 <br /> Comments <br /> *water and vapor samples and all TC-1 P&SPLP extracts are reported inµg/L,soil/sludge/solid samples inµg/kg, wipe samples in pg/wipe, <br /> product/otl/non-aqueous liquid samples in mg/L. <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysts <br /> #surrogate diluted out of range or surrogate coelutes with another peak <br /> h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than—2 vol %sediment,3)sample diluted due to high <br /> or anic content <br /> i <br /> f <br /> DHS Cenitiicapon No 1644 Angela Rydeltus, Lab Manager <br />