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110 2nd Avenue South,#137,Pacheco CA 94553-5560 <br /> McCatnpbell Analytical Inc Telephone 925-798-1620 Fax 925-798-1622 <br />' <br /> http//www tics bell com E-mail main mccan Abell corn <br /> • Advanced GeoEnvironmental,Inc Client Project ID Flag City Chevron Date Sampled 06/27/03 <br />' 837 Shaw Road Date Received 07/01/03 <br /> Client Contact Tim Cuellar Date Extracted 07104103-07/08103 <br /> Stockton,CA 95215 <br />' Client P O Date Analyzed 07/04/03-07/08/03 <br /> Oxygenates and BTEX by GC/MS* <br /> Extraction Method.SW5030B Analytical Method SW9260B Work Order 0307008 <br /> ILab ID 0307008-017B 0307008-018B 0307008-019B 0307008-020B <br /> Client ID MW13B MW13C MW13D MW11D <br /> Reporting Limit for <br />' Matrix W W W W DF=1 <br /> DF 1 1 1 �— 1 S W <br />' Compound Concentration ug/kgpg/L <br /> tert-Amyl methyl ether(TAME) ND ND ND ND NA 05 <br /> Benzene ND ND ND ND NA 05 <br /> t-Butyl alcohol(TBA) ND ND ND ND NA 50 <br /> Ditsopropyl ether(DiPE) ND ND ND ND NA 05 <br /> i <br /> Ethanol ND ND ND ND NA 50 <br /> I Ethylbenzene ND ND ND ND NA 0 5 <br /> Ethyl tert-butyl ether(ETRE) ND ND ND ND NA 05 <br /> Methanol ND ND ND ND NA 500 <br /> Methyl-t-butyl ether(MTBE) ND ND ND 2 1 NA 05 <br /> Toluene ND ND ND ND NA 05 <br /> Xylenes ND ND ND ND NA 05 <br /> Surrogate Recoveries(%} <br /> %SSI 111 116 110 113 <br /> %SS2 102 102 101 101 <br /> %SS3 104 102 105 103 <br /> Comments <br /> *water and vapor samples and all TCLP&SPLP extracts are reported in lig/L,soillsludge/solid samples inµg/kg, wipe samples inµg/wipe, <br /> product/oil/non-aqueous liquid samples in mg/L <br /> IND means not detected above the reporting limit,N/A means analyte not applicable to this analysts <br /> #surrogate diluted out of range or surrogate coelutes with another peals <br /> I h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than—2 vol %sediment,j)sample diluted due to high <br /> or ante content <br /> • <br /> 1 <br /> DHS Certification No 1644 Angela Rydehus, Lab Manager <br />