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110 2nd Avenue South,#137,Pacheco,CA 94553-5560 <br />' MCCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> h //www mccam bell com E-mail mam@mccampbell corn <br />' Advanced GeoEnvironmental Chent Project ID Flag City Chevron Date Sampled 09/06/01 <br /> 837 Shaw Road Date Received 09/07/01 <br />' Stockton, CA 95215 Client Contact Tim Cuellar Date Extracted 09/14/01 <br /> Client P O Date Analyzed 09/14/01 <br /> Seven Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br /> Lab ID 77244 77245 77246 77247 <br /> EW-4/ EW-5/ EW-6/ EW-7/ Reportmg Limit <br /> Client ID 09-06-01 09-06-01 09-06-01 09-06-01 <br /> Matrix W W W W S w <br /> Compound Concentration* ug/kg ug/L <br /> Di-isopropyl Ether(RIPE) ND ND ND ND 50 1 0 <br /> IEthyl tent-Butyl Ether(ETRE) ND ND ND ND 50 10 <br /> Methyl tert-Butyl Ether(MTBE) 14 35 12 ND 50 1 0 <br /> lie tert-Amyl Methyl Ether(TAME) ND ND ND ND 50 1 0 <br /> Itert-Butanol ND ND ND ND 25 50 <br /> IMethanol ND ND ND ND 2500 500 <br /> Ethanol ND ND ND ND 250 50 <br /> Surrogate Recoveries <br /> IDibromofluoromethane 99 101 102 101 <br /> IComments <br /> *water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/vinpe and all TCLP/STLC/SPLP extracts in ug/L <br /> D means not detected above the reporting limit,NIA means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present,(i)liquid sample that contains greater than—5 vol %sediment,0)sample diluted due to <br /> high organic content <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />