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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br />' MCCAWBELL ANALYTICAL INC tp//wTelephone 925-798-1620 Fax 925-798-1622 <br /> htww mccampbell cum E-mail main@mccampbell com <br />' Advanced GeoEnvironmental Client Project ID Flag City Date Sampled 09/07/01 <br /> 837 Shaw Road Date Received 09/07/01 <br />' Stockton, CA 95215 Client Contact Tun Cuellar Date Extracted 09/14-09/22101 <br /> Client P 0 Date Analyzed 09/14-09122101 <br />' Seven Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br />' Lab ID 77360 77361 1 77362 77363 <br /> MW l if)/ MW 12A/ M W 12B/ MW 12C/ Reporting Limit <br /> Client ID 09070I 090701 090701 090701 <br /> Matrix W WW W S W <br /> Compound Concentration* ug/kg ug/L <br /> Di-isopropyl Ether(RIPE) ND ND ND ND 50 10 <br /> Ethyl tert-Butyl Ether(ETBE) ND ND ND ND 50 10 <br /> Methyl tert-Butyl Ether(MTBE) ND ND ND ND 50 to <br /> tent-Amyl Methyl Ether(TAME) ND ND ND ND 50 to <br /> tert-Butanol ND ND ND ND 25 so <br /> Methanol ND ND ND ND 2500 500 <br /> Ethanol ND ND ND ND 250 50 <br /> Surrogate Recoveries(%) <br /> Dibromofluoromethane 105 105 105 102 <br /> Comments <br /> *water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/STLC 13PLP extracts in ug/L. <br /> ND means not detected above the reporting limit,N/A means surrogate not applicable to this analysis <br /> (h)lighter than water imrruscible sheen is present,(i)liquid sample that contains greater than—5 vol %sediment,0)sample diluted due to <br /> high organic content <br /> I <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />