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110 2nd Avenue South #D7 Pacheco CA 94553-5560 <br /> - McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> h //www mccam bell corn E-mail main@mccampbell corn <br /> Advanced GeoEnvironinental Client Protect ID Flag City Chevron Date Sampled 03/08/01 <br /> 837 Shaw Road Date Receivers 03/09/01 <br /> Stockton, CA 95215 Client Contact Tim Cuellar Date Extracted 03/11-03/15/01 <br /> Client P O Date Analyzed 03/11-03/15/01 <br /> I7 Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br />' Lab 1D 62013 62014 62015 62016 <br /> MWI/ MW2/ MW4/ MW5/ Reporting Limit <br /> Client 1D 03-08-01 03-08-01 03-08-01 03-08-01 <br /> Matrix W W W W S w <br /> Compound Concentration* ug/kg ug/L <br /> Di-isopropyl Ether(DIPS) ND<2 5 ND ND ND 50 10 <br /> Ethyl tert-Butyl Ether(ETBE) ND<2 5 ND ND ND 50 10 <br /> Methyl-tert Butyl Ether(MTBE) 120 ND ND ND 50 10 <br /> lie <br /> tert-Amyl Methyl Ether(TAME) ND<2 5 ND ND ND 50 10 <br /> tent-Butanol ND<12 5 ND ND ND 25 50 <br /> Methanol N13<2000 ND ND ND 1000 200 <br /> Ethanol ND<500 ND ND ND 25D 50 <br /> Surrogate Recoveries(%) <br /> Dibromofluoromethane 110 106 108 108 <br /> Comments <br /> *water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/STLC/SPLP extracts in ug/L <br /> IND means not detected above the reporting limit,N/A means surrogate not applicable to this analysis <br /> (h)lighter than water imtitiscible sheen is present,(i)liquid sample that contains greater than—5 vol %sediment,0)sample diluted due to <br /> high organic content <br /> I <br /> DHS Certification,No 1644 Edward Hamilton, Lab Director <br />