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f <br /> I 10 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> 4 McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> http//www mccampbell com E-mail main@mccampbell corn <br /> Advanced GeoEnvironmental Client Project ID Flag City Chevron Date Sampled 03/08/01 <br /> 837 Shaw Road Date Received 03/09/01 <br />' Stockton,CA 95215 Client Contact Tim Cuellar Date Extracted 03/11-03/15/01 <br />' Client P O Date Analyzed 03111-03/15/01 <br /> _J - <br /> 7 Oxygenated Volatile Organics By GUMS <br /> EPA method 8260 modified <br />' Lab ID 62029 62030 62031 62032 <br /> EW6/ EW7/ EW8/ EW9/ Reporting Limit <br /> Client ID 03-08-01 03-08-01 03-08-01 03-08-01 <br />' Matrix W W W W S W <br /> Compound Concentration* uglkg ug/L <br />' <br /> Di-isopropyl Ether(DIPE) ND ND ND ND 50 i 0 <br />' Ethyl tert-Butyl Ether(ETRE) ND ND ND ND 50 10 <br />' • Methyl-tert Butyl Ether(MT131:) 46 42 27 49 50 10 <br /> tert-Amyl Methyl Ether(TAME) ND ND ND ND 50 to <br /> tert-Butanol ND ND ND ND 25 50 <br />' Methanol ND ND ND ND 1000 200 <br />' Ethanol ND ND ND ND 250 50 <br /> Surrogate Recoveries(%) <br /> 1 <br /> Dibromofluoremethane 110 109 109 1 I O <br /> Comments <br />' *water samples ate reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP I STLC 1 SPLP extracts in ug/L <br /> ND means not detected above the reporting limit,NIA means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present (i)liquid sample that contains greater than—5 vol %sediment 0)sample diluted due to <br />' high organic content <br /> 1 <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br /> 1 <br /> i <br />