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1 q <br /> I 10 2nd Avenue South,#D7, Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> http//wwwmccampbellco E-mail main@mccampbell com <br /> Date Sampled 03/27-03128/02 <br /> Advanced GeoEnvirotimental Client Project ID Flag City <br /> 837 Shaw Road Date Received 03/28/02 <br /> Stockton, CA 95215 CIient Contact Tim Cuellar Date Extracted 03/28/02 <br /> Client P O Date Analyzed 03/29-04/01102 <br /> CAM/CCR 17 Metals* <br /> EPA methods 6010/200 7,7470/7471/245 1/245 5(Hg),7060/206 2(As) 7740/270 2(Se),7841/279 2(Tl),239 2(Pb,w) 204 2(Sb,w) <br /> Lab ID 0203513-035 <br /> Reporting Limit <br /> Client ID EFFLUENT <br /> Matrix W S W STLC <br /> Extraction° TTLC TTLC TTLC TCLP <br /> Compound Concentration' mg/kg mg/L mg/L <br /> Antimony(Sb) ND 25 0 006 <br /> 07 05 <br /> Arsenic(As) ND 25 0 005 025 <br /> Barium(Ba) <br /> 012 25 005 005 <br /> Beryllium(Be) ND 05 0 004 001 <br /> Cadmium(Cd) ND 05 0 005 001 <br /> Chromium(Cr) ND 05 002 005 <br /> Cobalt(Co) ND 20 005 005 <br /> Copper(Cu) ND 20 005 005 <br /> Lead(Pb) ND 30 0 005 02 <br /> Mercury(Hg) ND 006 00008 0 005 <br /> Molybdenum(Mo) ND 25 005 0 05 <br /> Nickel(Ni) ND 20 005 005 <br /> Selenium(Se) ND 25 0 005 025 <br /> Silver(Ag) ND to 001 005 <br /> Thallium(Tl) ND 25 0 005 05 <br /> Vanadium(V) ND 20 005 005 <br /> Zinc(Zn) ND 10 005 005 <br /> %Recovery Surrogate <br /> Comments <br /> 'water samples are reported in mg/L,soil and sludge samples in mg/kg,wipes in ug/wipe and all TCLP/STLC/SPLP extracts in mg/L <br /> ND means not detected above the reporting limit,N/A means surrogate not applicable to this analysis <br /> °EPA extraction methods 1311(TCLP),3010/3020(water,TTLC),3040(organic matrices,TTLC),3050(solids,TTLC),STLC-CA Title 22 <br /> DISTLC extractions are performed using STLC methodology except that deionized water is substituted for citric acid buffer as the <br /> extraction fluid D151 LC results are not applicable to STLC regulatory limits <br /> "surrogate diluted out of range <br /> reporting limit raised due to matrix interference <br /> 1) liquid sample that contains greater than —2 vol % sediment this sediment i extracted with the liquid, in accordance with EPA <br /> methodologies and can significantly effect reported metal concentrations <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />