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I <br /> 110 2nd Avenue South,#137,Pacheco, CA 94553-5560 <br /> McCAWBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> http//www mccampbell cam E-mail main@mccampbell com <br /> i <br /> Advanced GeoEnvtronmental Client Project ID Flag City Cheveron Date Sampled 03/31/02&04/02/02 <br /> 837 Shaw Road Date Received 04/01/02&04103/02 <br /> Stockton, CA 95215 CIient Contact Tun Cuellar Date Extracted 04/03/02 <br /> Client P O Date Analyzed 04/05/02 <br /> Chlorinated Pesticides(including PCBs) <br /> EPA method 608 and 3510 or 8080 and 3550 <br /> Lab ID 0204071 Reporting Limit <br /> Client ID EFFLUENT W,STLC, <br /> S <br /> Matrix W TCLP <br /> Compound Concentration* ug/kg ug/L <br /> Aldnn ND 10 0 005 <br /> cc-BHC ND 10 001 <br /> R-BHC ND 10 0 005 <br /> y-BHC(Lindane) ND 10 002 <br /> cr-BHC ND 10 0 005 <br /> Chlordane ND 10 01 <br /> p,p-DDD(k) ND 10 005 <br /> p,p-DDE(k) ND 10 005 <br /> p,p-DD'Tlkl ND 10 001 <br /> Dieldrin ND 10 001 <br /> Endosulfan I ND 10 002 <br /> Endosulfan 11 ND 10 001 <br /> Endosulfan Sulfate ND 10 005 <br /> Endrin ND 10 001 <br /> Endrin Aldehyde ND 10 001 <br /> Heptachlor ND 10 001 <br /> Heptachlor Epoxide ND 10 001 <br /> p,p'-Methoxychlor*) ND 10 to <br /> PCB-Total(+) ND 50 05 <br /> Toxaphene ND 100 05 <br /> %Recovery Surrogate 114 <br /> Comments I L <br /> *water and vapor samples are reported in ug/L,oils in mg/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP <br /> extracts in ug/L <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> "surrogate diluted out of range or surrogate coelutes with another peak <br /> `(a)PCS aroclor 1016,(b)PCB aroclor 1221,(c)PCS aroclor 1232,(d)PCB aroclor 1242,(e)PCB aroclor 1248,(f)PCB aroclar 1254,(g) <br /> PCB aroclor 1260, (h)a lighter than water irrsmscrble sheen is present, (i)liquid sample that contains >--5 vol %sediment, 0)sample <br /> diluted due to high organic content,(k)p,p-is the same as 4,4'-, (1)ftonsil(EPA 3 0)cleanup,(m)silica-gel(EPA 3630)cleanup <br /> DIJS Certification No 1644 Edward Hamilton,Lab Director <br />