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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> 4 MCCANIPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> http//u-ww mccarnybell com E-mail mam c mccampbell com <br /> Advanced GeoEnvironmental Client Protect ID Flag City Date Sampled- 05108-05/09/00 <br /> 4005 North Wilson Way Date Received 05/11/00 <br /> Stockton, CA 95205 Client Contact Tim Cuellar Date Extracted 05/11-05/17/00 <br /> Client P O Date Analyzed 05/15-05/17/00 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab 1D 37536 <br /> Client 1D P-28-W <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br /> Acetone`b' --- trans-1,3-Dichloropropene --- <br /> Benzene TD Eth,,ierie dibrom:de --- <br /> Bromobenzene -- Eth�,lbenzene ND <br /> Bromochloromethane --- Hexachlorobutadiene <br /> Bromod:chloromeihane --- Iodomethane --- <br /> Bromoform --- Isopropylbenzene — <br /> Bromomethane -- p-Isopropyl toluene --- <br /> n-Butyl benzene --- Meth)]burvl ketone' --- <br /> sec-But)]benzene --- Methylene Chloride"' <br /> Cert-Butyl benzene --- Methyl eth)1 ketone ' -- <br /> Carbon Disulfide -- Meth}]isobunI ketone r --- <br /> Carbon Tetmchlonde - Mcthyl tert-Butyl Ether(MTBE) -- <br /> Chlorobenzene 'Naphthalene --- <br /> . Chloroethane " n Propyl benzene <br /> 2-Chloroethyl Vinyl Ether" sr+-ene"I <br /> Chloroform --- 1,1,12-Tetrachloroethane --- <br /> Chloromethane 1 1 2,2-Tetrachloroethane --- <br /> 2-Chlorotoluene Tetrachloroethene --- <br /> 4-Chlorotoluene Toluene'' ND <br /> Dibromochloromethane 1,2 3-Tr:chlorobenzene --- <br /> 1,2 D:bromo-3-chloroprop2ne 1,2 4 Tnchlorobenzene --- <br /> D:bromomethane 1,1 1 Trichloroethane -- <br /> 1,2-Dichlorobenzene --- 1,12-Trichloroethane --- <br /> 1,3 Dichlorobenzene Tnchloroethene <br /> 1,4-Dichlorobenzene TnChl0T0flU0r0meth2ne -- <br /> Dichlorodifluoromethane 1,2,3 Tnchloropropane -- <br /> ],]-Dichloroethane 1 2 4-Trlmeih\lbenzene --- <br /> 42-D:chloroethane 1 3 5 Trimetli)lbenzene --- <br /> 3,1-Dichloroethene --- Vim]Acetate - <br /> cis-1,2-Dichloroethene \im 1 Chloride -- <br /> trans 1,2-Dichloroethene Wenes,total ND <br /> 1,2 Dichloropropane --- Comments i <br /> 1,3 Dichloropropane - Surrogate 12ecorcries(%) <br /> 2,2-Dichloropropane --- Dibrom:oilueromethane 126 <br /> 1,1-Dic17110ropropenc Toluene-ds 109 <br /> cis-] 3 Dichloropropene -- 4-Bromoiluorobenzene 94 <br /> water and,.apor samples are repotted ri ug L soil and sludge samples in ug/kg,wipes in ug'w 1pe and all TCLP/SPLA extracts in ug/L <br /> Reporting limits unless vihcm isc stated eater samples 1 ug/L %apor samples 0 5 ugIL,solid and sludge samples 5 ug/kg,,A ipes 0 2ugl%%ipe <br /> ND means not detected above the reporting limit N/A means anal)te not applicable to this anal)sis <br /> (b) 2 propanone or dimethvl ketone (c) (_-chloroethoay)ethene, (d) 2 hexanone, (e) dichloromethane, (f) 2-butanone, (g)4-meth)]-2 <br /> penianone or:soprop\lacetone, (h) lighter than water immiscible sheen is present,())liquid ,amplc that contains greater than—5 -.ol % <br />• <br /> sediment, (t) sample diluted due to h:ch organic content, (k) ethem)benzene (I meihNlbcnzcne, (m) acetic acid ethcn,,l ester, (n) <br /> chloroethene (o)dimcih-lbenzenes <br /> DHS Certification No 1644 Edv.and Hamilton, Lab Director <br />