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i <br />' 110 Second Avenue South,#D7,Pacheco,CA 94553-5560 <br /> MCCAWBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> IhnpJlNnww_mco1npbell com E-mail main@mccampbell com <br /> Advanced GeoEnvironmental Client Project ID Flag City Chevron Date Sampled 02/25/99 <br /> 4005 North Wilson Way <br /> Date Received 03/03/99 <br />' Stockton,CA 95205 Client Contact Tun Cuellar Date Extracted 03/04-03/05/99 <br /> Client P O Date Analyzed 03/04-03/05/99 <br />' Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br /> Lab ID 04260 04261 04262 <br />' <br /> Client ID MW-6A/ MW-613/ MW-71 Reporting Limit <br /> 2-25-99 2-25-99 2-25-99 <br /> Matrix W W W S W <br /> Compound Concentration* ug/kg ug/L <br /> Di-isopropyl Ether(DIPS) NO ND NO 50 10 <br /> Ethyl tert-Butyl Ether(ETBE) NO NO NO 50 10 <br /> Methyl-tert Butyl Ether(MTBE) 3 2 3 5 33 50 10 <br /> tert-Amyl Methyl Ether(TAME) ND ND NO 50 1 0 <br /> tert-Butanol ND NO NO 25 50 M <br /> ISurrogate Recoveries(%) <br /> Dtbromotluoromethane 94 95 92 <br /> Comments <br /> *water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/STLC/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit,N/A means surrogate not applicable to this analysts <br /> I (h)lighter than water immiscible sheen is present,(i)liquid sample that contains greater than--5 vol %sediment,0)sample diluted due to <br /> high organic content <br /> DHS Certification No 1644 //V Edward Hamilton,Lab Director <br /> I <br />