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E. - - <br /> 1 10 Second Avenue South,#fD7,Pacheco;CA 94553 <br /> McCAMPBELL ANALYTICAL INC. Telephone: 510-798-1620 Fax :510-798-1622 <br /> i- http://www.niccampbell.com E-mail: main@mccampbell.com <br /> T <br /> Advanced GeoEnvironmental Client Project ID: Flag City Chevron Date Sampled: 08/29/97 <br /> 1803 West March Lane, Ste A <br /> Date Received: 09/05/97 <br /> Stockton,CA 95207 Client Contact: Tim Cuellar Date Extracted: 09/05/97 <br /> Client P.O: Date Analyzed: 09/05/97 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 50500 <br /> Client ID P3-20 <br /> Matrix S <br /> Compound Concentration* Compound Concentration* <br /> AcetoneND Iran s-1,3-Dichloropropene ND <br /> Benzene ND Ethylene dibromide` ' ND <br /> Bromobenzene ND Ethylbenzene ND <br /> Bromochloromethane ND Hex ac hlorobutad iene ND <br /> Bromodichloromethane ND lodomethane ND <br /> A Bromoform ND lsopropylbenzene ND <br /> Bromomethane ND p-Isopropyl toluene ND <br /> n-Butyl benzene ND Methyl butyl ketone"' ND <br /> sec-Butyl benzene ND Methylene Chloride" ND <br /> t tent-Butyl benzene ND Methyl ethyl ketone'r' ND <br /> Carbon Disulfide ND Methyl isobutyl ketone' ' ND <br /> Carbon Tetrachloride ND Methyl tert-Butyl Ether(MT13F) ND <br /> Chlorobenzene ND Napthalene ND <br /> Chloroethane ND n-Propyl benzene ND <br /> 2-Chloroethyl Vinyl Ether" ND Styrene` ND <br /> Chloroform IT'D 1,1,1,2-'I-etrachloinctliane ND <br /> Chloromethane ND 1,1,2,2-Tetrachloroethane ND <br /> 2-Chlorotoluene ND Tetrachloroethene ND <br /> 4-Chlorotoluene ND Toluene""' ND <br /> Dibromochloromethane ND 1,2,3-Trichlorobenzerne ND <br /> 1,2-Dibromo-3-cltloropropane ND 1,2,4-Trichlorobenzene ND <br /> Dibromomethane ND 1,1,1-Trichloroethane ND <br /> 1,2-Dichlorobenzene ND 1,1,2-Trichloroethane ND <br /> 1,3-Dichlorobenzene ND Trichloroethene ND <br /> 1,4-Dichlorobenzene ND Trlchl01'011LI01'Omethane ND <br /> Dichlorodifluoromethane ND 1,2,3-Trichloropropane ND <br /> 1,1-Dichloroethane ND 1,2,4-Trimethylbenzene ND <br /> F 1,2-Dichlaroethane ND 1,3,5-Trimethylbenzene ND <br /> [,1-Dichloroethene ND Vinyl Acetate"" ND <br /> cis-1,2-Dichloroethene ND Vinyl Chloride`"' ND { <br /> trans-1,2-Dichloroethene ND Xylenes,total 'n' ND 1 <br /> 1,2-Dichloropropene ND Comments: <br /> 1,3-Dichloropropane ND Surrogate Recoveries("/„) <br /> F 2,2-Dichloropropane ND Dibrontotluoromethane 107 <br /> 1,1-Dichloropropene ND Toluene-d8 105 <br /> cis-1,3-Dichloropropene ND 4-Bronloflnorobenzene 98 <br /> 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP I SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated:water samples 1 ug/L;vapor samples 0.5 ug/L;solid and sludge samples 5 ug/kg;wipes 0.2ug/wipe <br /> ND means not detected above the reporting limit;N/A means analyte not applicable to this analysis <br /> ► (b) 2-propanone or dimethyl ketone; (c)(2-chloroethoxy) ethene; (d) 2-11exannne; (e) dichloromethane; (f) 2-butanone; (g) 4-methyl-2- <br /> pentanone or isopropylacetone; (h) lighter than water immiscible sheen is present; (i) liquid sample that contains greater than —5 vol. % <br /> sediment; (j) sample diluted due to high organic content; (k) ethenylbenzene; (1) methylbenzene; (mm) acetic acid ethenyl ester; (n) <br /> chloroethene;(o)dimethylbenzenes. <br /> r DHS Certification No. 1644 xAl Edward Hamilton,Lab Director <br />