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r— i . I � 110 Second Avenue South,#D7, Pacheco,CA 94553 McCAMPBELL ANALYTICAL INC. Telephone:510-798-1620 Fax :510-798-1622 http://www.mccaiiipbe[l.cont E-mail:main@mccampbell.com ► } Advanced GeoEnvironmental Client Project 1D: Flag City Chevron Date Sampled: 08/29/97 1803 West March Lane, Ste A Date Received: 09/05/97 Stockton,CA 95207 Client Contact: Tim Cuellar Date Extracted: 09/05/97 Client P.O: Date Analyzed: 09/05/97 Volatile Organics By GC/MS EPA method 8260 Lab ID 80513 Client ID P3-57 Matrix S Compound Concentration* Connpound Concentration* Acetone" ND trans-1,3-Dichloropropene ND Benzene ND Ethylene dibromide' ' ND Bromobenzene ND Ethylbenzene ND Bromochloromethane ND Hex achlorobutadiene ND Bromodichloromethane ND lodomethane ND Bromoform ND Isopropylbenzene ND Bromomethane N'D p-Isopropyl toluene ND n-Butyl benzene ND Methyl butyl ketone"' ND sec-Butyl benzene ND Nlethylene Chloride" ND teri-Butyl benzene ND Methyl ethyl ketone'"' ND Carbon Disulfide ND Methyl isobutyl ketone` ' ND Carbon Tetrachioride ND Methyl tert-Butyl Ether(MTBE) ND Chlorobenzene ND Napthalene ND Chloroethane ND n-Propyl benzene ND 2-Chloroethyl Vinyl Ether" ND Styrene" ND r—^ Chloroform ND 1,1,1,2-Tetrachloroethane ND (: t Chloromethane ND 1,1,2,2-Teurachloroethane ND r a 2-Chlurotoluene ND Tetrachlorocthene ND I 4-Chlorotoluene ND Toluene'"' ND Dibromochloromethane ND 1,2,3-Trichlorobcnzene ND 1,2-Dibromo-3-chloropropane ND 1,2,4-1'richlorobenzene ND Dibromomethane ND 1.1.1-Trichloroethane ND 1,2-Dichlorobenzene ND 1,1,2-Trichloroethane ND 1,3-Dichlorobenzene ND Trichlornelhcne ND 1,4-Dichlorobenzene ND Trichlorotluoromethane ND Dichlorodifluoromethane ND 1,2,3-Trichloropropane ND l,l-Dichloroethane ND 1.2,4-'frimethylbenzene ND 1,2-Dichloroethane ND 13,52Trimethy1benzene ND 1,1-Dichloroethene ND Vinyl Acetate"" ND cis-1,2-Dichloroethene ND Vinyl Chloride'°" ND trans-l,2-Dichloroethene ND Xylenes,total ND 1,2-Dichloropropane ND Comments: 1,3-Dichloropropane ND Surrogate Recoveries(1/4) 2,2-Dichloropropane ND Dibromnlluoromethane 95 1,1-Dichloropropene ND Toluene-dS 106 cis-1,3-Dichloropropene ND 4-13ronOtlLlorobenzene 96 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L Reporting limits unless otherwise stated:water samples 1 ug/L;vapor samples 0.5 ug/L;solid and sludge samples 5 ug/kg;wipes 0.2ug/wipe ND means not detected above the reporting limit;NLA means analyte not applicable to this analysis D (b) 2-propanone or dimethyl ketone; (c) (2-chloroethoxy) ethene; (d) 2-1cxanooc; (c) dichloromethane; (t) 2-butanone; (g) 4-methyl-2- pentanone or isopropylaeetone; (h)lighter than water immiscible sheen is present; (i)liquid sample that contains greater than --5 vol. % sediment; 0) sample diluted due to high organic content; (k) ethenylbenzene; (1) methylbenzene; (m) acetic acid ethenyl ester; (n) ' chloroethene;(o)dimethylbenzenes. i DHS Certification No. 1644 /� Edward Hamilton,Lab Director E .