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E 10 Second Avenue South,#137,Pacheco,CA 94553 <br /> MCCAMPBELL ANALYTICAL INC. Telephone : 510-798-1620 Fax :510-798-1622 <br /> httpa/www.mccampbcll.cotn E-mail: main@mccampbell.com <br /> Advanced GeoEnvironmental Client Project 1D: Flag City Chevron Date Sampled: 08/29/97 <br /> 1803 West March Lane, Ste A Date Received: 09/05/97 <br /> Stockton, CA 95207 Client Contact: Tim Cuellar Date Extracted: 09/05/97 <br /> Client P.O: Date Analyzed: 09/05/97 <br /> Oxygenated Volatile Organics By GC/1135 <br /> EPA method 8260 modified <br /> Lab ID 80500 50508 50513 <br /> Reporting Limit <br /> Client ID P3-20 P3-37 P3-57 <br /> Matrix S S S S w <br /> Compound Concentration* ug/kg ug/L <br /> IDi-isopropyl Ether(RIPE) ND ND ND 5.0 1.0 <br /> Ethanol --- --- --- --- 100 20 <br /> Ethyl tert-Butyl Ether(ETRE) ND ND ND 5.0 1.0 <br /> Methanol -- --- --- --- N/A N/A <br /> Methyl-tert Butyl Ether(MTBE) ND ND ND 50 5.0 <br /> Cert-Amyl Methyl Ether(TAME) ND ND ND 5.0 1.0 <br /> tert-Butanol ND ND ND 25 5.0 <br />' Surrogate Recoveries('X.) <br /> Dibromotluoromethane 107 102 95 <br /> Toluene-dg 105 103 106 <br /> Comments: <br />' *water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/STLC/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit;N/A means swTogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present;(i)liquid sample that contains greater than—5 vo€.°/sediment;0)sample diluted due to <br /> high organic content <br /> DHS Certification No. 1644 / Edward Hamilton,Lab Director <br />