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I 10 Second Avenue South,#iD7,Pacheco,CA 94553 <br /> McCAMPBELL ANALYTICAL INC. Telephone : 510-798-1620 Fax:510-798-1622 <br /> lilt p:/hvww.mccampbell.corn E-mail: main@mccampbell.com <br /> mccampbell.com <br /> IAdvanced GeoEnvironmental Client Project ID: Flag City Chevron Date Sampled: 09/05/97 <br /> Date Received: 09/09/97 <br /> 1803 West March Lane, Ste A <br /> Stockton, CA 95207 Client Contact: Tim Cuellar Date Extracted: 09/09-09/10/97 <br /> Client P.O: Date Analyzed: 09/09-09/10/97 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 80568 <br /> Client ID P4/51'-56' <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br /> I Acetone' ' ND<2 trans-1,3-Dichloropropene ND <br /> Benzene ND Ethylene dibromide' ' ND <br /> BrOmoben Zene ND Ethyibenzene ND <br /> Bromochloromethane ND HexachlorobtrladienC ND <br />' Bromodichloromethane ND lodomethane ND <br /> Bromoform ND lsopropylbenzene ND <br /> Bromotnethane ND p-Isopropyl toluene ND <br /> n-Butyl benzene ND Methyl butyl ketone"' ND <br />' sec-Butyl benzene ND Methylene Chloride" N'D <br /> tent-Butyl benzene ND Methyl ethyl ketone'' ND <br /> Carbon Disulfide ND Methyl isobutyl ketone` ' ND <br /> Carbon Tetrachloride ND Methyl tert-Butyl Ether(MTBE) --- <br /> Cltlorobenzene ND Naptbalene ND <br /> Chloroethane ND n-Propyl benzene ND <br /> 2-Chloroethyl Vinyl Ether" ND Styrene"I ND <br /> Chloroform ND 1,1,1,2-Tetrachloroethane ND <br /> Chloromethane ND 1,1,2,2-Tetrachloroethane ND <br /> 2-Chlorotoluene ND Torachloroethene ND <br /> 4-Chlorotoluene ND Toluene""' ND <br /> Dibromochloromethane ND 1,2,3-Trichlorobenzene ND <br /> 1,2-Dibromo-3-chloropropane ND 1,2,4-Trichlorobenzene ND <br /> Dibromomethane ND l,l,l-Trichloroctlhane ND <br /> 1,2-Dichlorobenzene ND 1,1.2-'Crichlomethane ND <br /> 1,3-Dichlorobenzene ND Trichloroethene ND <br /> 1,4-Dichlorobenzene ND Trichlorofluoromethane ND <br /> Dichlorodifluoromethane ND 1,2,3-Trichloropropane ND <br /> 1,1-Dichloroethane ND 1,2,4-37imethylbenzene ND <br /> 1,2-Dichloroethane ND 1,3,5-Trimethylbenzene ND <br /> ],I-Dichloroethene ND Vinyl Acetate"" ND <br /> cis-1,2-Dichloroethene ND Vinyl Chloride"' ND <br /> trans-1,2-Dichloroethene ND Xylenes,total "' ND <br />' 1,2-Dichloropropane ND Comments:i <br /> 1,3-Dichloropropane ND Surrogate Recoveries('%,) <br /> 2,2-Dichloropropane ND Dibromotlucnnmethane 92 <br /> 1,1-Di chloropropene ND Toluene-dg 109 <br /> cis-1,3-Dichloropropene ND 4-13romGluorobenzene 93 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated:water samples 1 ug/L;vapor samples 0.5 ug/L;solid and sludge samples 5 ug/kg;wipes 0.2ug/wipe <br /> ND means not detected above the reporting limit;NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone; (c) (2-chloroethoxy) ethene; (d) 2-hexanone; (e) dichloromethane; (f) 2-butanone; (g) 4-methyl-2- <br /> pentanone or i sopropyl acetone; (h)lighter than water immiscible sheen is present; (i) liquid sample that contains greater than —5 vol. °/U <br /> sediment; 6) sample diluted due to high organic content; (k) ethenylbenzene; (1) methylbenzene; (m) acetic acid ethenyl ester; (n) <br /> chloroethene;(o)dimethylbenzenes. <br /> DHS Certification No. 1644 /5' Edward Hamilton,Lab Director <br />