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I 10 Second Avenue South,#D7, Pacheco,CA 94553 <br /> McCAMPBELL ANALYTICAL INC. Telephone : 510-798-1620 Fax : 510-798-1622 <br /> http://w%vw.mccanil)bell.com E-mail:main@mccampbell.com <br /> Advanced GeoEnvironmental Client Project ID: Flag City Chevron Date Sampled: 09/22/97 <br /> Date Received: 09/24/97 <br /> 1803 West March Lane, Ste A <br /> Stockton, CA 95207 Client Contact: Tim Cuellar Date Extracted: 09/24/97 <br /> Client P.O: Date Analyzed: 09/24/97 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 81101 <br /> Client 1D P 10-45 <br /> Matrix S <br /> Compound Concentration* Compound Concentration* <br /> Acetone` ' ND<6 trans-1,3-Dichloropropene ND <br /> Benzene ND Ethylene dibromide' ' ND <br /> Bromobenzene ND Ethylbenzene ND <br /> Bromochloromethane ND HexachlOTobinadiene ND <br /> Bromodichloromethane ND lodomethane ND <br /> Bromoform ND lsopropylbenzene ND <br /> Bromomethane ND p-Isopropyl toluene ND <br /> n-Butyl benzene ND Methyl butyl ketone"' ND <br /> sec-Butyl benzene ND Methylene Chloride"' ND <br /> tert-Butyl benzene ND Methyl ethyl ketone" ND <br /> Carbon Disulfide ND Methyl isobutyl ketone` ' ND <br /> Carbon Tetrachloride ND Methyl tort-Butyl Ether(Ml'BE) <br /> Chlorobenzene ND Napthalene ND <br /> Chloroethane ND n-Propyl benzene ND <br /> 2-Chloroethyl Vinyl Ether` ND Styrene' ND <br /> Chloroform ND 1,1,1,2-Tetrachloroethane ND <br /> Chloromethane ND 1,1,2,2-Tetrachloroethane ND <br /> 2-Chlorotoluene ND Tetrachloroethene ND <br /> 4-Chlorotoluene ND Toluene") ND <br /> Dibromochloromethane ND 1,2,3-Trichlorobenzene ND <br /> 1,2-Dibromo-3-chloropropane ND 1,2,4-Trichlorobenzene ND <br /> Dibromomethane ND 1,1,1-Trichloroethane ND <br /> 1,2-Dichlorobenzene ND 1,1,2-Trichtoroethane ND <br /> 1,3-Dichlorobenzene ND Trichloroethene ND <br /> 1,4-Dichlorobenzene ND TriCiIiOTOt loronlethane ND <br /> Dichlorodifluoromethane ND 1,2,3-Trichtoropropane ND <br /> 1,1-Dichloroethane ND 1,2,4-Trimethylbenzene ND <br /> 1,2-Dichloroethane ND 1,3,5-Trimethylbenzene ND <br /> l,]-Dichloroethene ND Vinyl Acetate"" ND <br /> cis-1,2-Dichloroethene ND Vinyl Chloride"" ND <br /> vans-1,2-Dichloroethene ND Xylenes,total 'r' ND <br /> 1,2-Dichloropropane ND Comments: <br /> 1,3-Dichloropropane ND Surrogate Recoveries <br /> 2,2-Dichloropropane ND Dibromotlltol"olllethalle 95 <br /> 1,1-Dichloropropene ND Toluene-d8 102 <br /> cis-1,3-Di chloropropene ND 4-Brom0iluorobenzene 94 <br /> `water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP I SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated:water samples 1 ug/L;%,apor samples 0.5 ug/L;solid and sludge samples 5 ug/kg;wipes 0.2uglwipe <br /> ND means not detected above the reporting limit;NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone; (c) (2-chloroethoxy) ethene; (d) 2-hexanone; (e) dichloromethane; (f) 2-butanone; (g) 4-methyl-2- <br /> pentanone or isopropylacetone; (h)lighter than water immiscible sheen is present; (i) liquid sample that contains greater than --5 vol. % <br /> sediment; 6) sample diluted due to high organic content; (k) ethenylbenzene; (1) methylbenzene; (m) acetic acid ethenyl ester; (n) <br /> cbloroethene;(o)dimethylbenzenes. <br /> DHS Certification No. 1644 Edward Hamilton,Lab Director <br />