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I 10 Second Avenue South,#D7,Pacheco,CA 94553 <br /> MCCAMPBELL ANALYTICAL INC. Telephone: 510-798-1620 Fax : 510-798-1622 <br /> 24http://wNvw.mccampbell.com E-mail: main@mccampbell.com <br />' Advanced GeoEnvironmental Client Project ID: Flag City Chevron Date Sampled: 09/22/97 <br /> Date Received. 09/24/97 <br />' 1803 West March Lane, Ste A <br /> Stockton, CA 95207 Client Contact: Tim Cuellar Date Extracted: 09126-09/30/97 <br /> Client P.O: Date Analyzed: 09126-09/30/97 <br />' Volatile Organics By GC/i•'IS <br /> EPA method 8260 <br />' Lab ID 81105 <br /> Client 1D P14/51-55m <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br />' Acetone` ND<4.5 trans-l,3-Dichloropropene ND <br /> Benzene ND Ethylene dibromide` ' ND <br /> Bromobenzene ND Ethylbenzene ND <br /> Bromochloromethane ND Hexachlorobutadiene ND <br />' Bromodichloromethane ND lodomethane ND <br /> Bromoform ND lsopropylbenzene ND <br /> Bromomethane ND p-Isopropyl toluene ND <br /> n-Butyl benzene ND Methyl butyl ketone"' ND <br />' sec-Butyl benzene ND Methylene Chloride" ND <br /> Cert-Butyl benzene ND Methyl ethyl ketone"' ND <br /> Carbon Disulfide ND Methyl isobutyl ketone' ' ND <br /> Carbon Tetrachloride ND Methyl tert-Butyl Ether(MTBE) <br /> Chlorobenzene ND Napthalene ND <br /> Chloroethane ND n-Propyl benzene ND <br /> 2-C}tloroethyl Vinyl Ether` ND Styrene" ND <br /> Chloroform ND 1,1,1,2-Tetrachloroethane ND <br /> Chloromethane ND 1,1.2,2-Tetrachloroethane ND <br /> 2-Chlorotoluene ND Tetrachlorocthene ND <br /> 4-Chlorotoluene ND Toluene ND <br /> Dibromochloromethane ND 1,23-Trichlorobenzene ND <br /> 1,2-Dibromo-3-chlompropane ND 1,2,4-Trichlorobenzene ND <br /> Dibromomethane ND 1,1,1-'Frichloroethane ND <br /> 1,2-Dichlorobenzene ND 1,1,2-Trichloroethane ND <br /> 1,3-Dichlorobenzene ND Trichloroethene ND <br />' 1,4-Dichlorobenzene ND TrichlorotluOrOmetllane ND <br /> Dichlorodifluoromethane ND 1,2,3-Trichloropropane ND <br /> 1,1-Dichloroethane ND 1,2,4-Trimethylbenzene ND <br /> 1,2-Dichloroethane ND 1,3,5-Trimethylbenzene ND <br />' 1,1-Dichloroethene ND Vinyl Acetate"" ND <br /> cis-1,2-Dichloroethene ND Vinyl Chloride'°' ND <br /> trans-1,2-Dichloroethene ND Xylenes,total `u' ND <br /> 1,2-Dichloropropane ND Commentsd <br /> 1,3-Dichloropropane ND Surrogate Recoveries('%) <br /> 2,2-Dichloropropane ND Dibromoiluoromethane 96 <br /> 1,1-Dichloropropene ND Totuene-d8 94 <br />' cis-1,3-Dichloropropene ND 4-Bromoiluorobenzene &7 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP 1 SPLP extracts in uglL <br /> Reporting limits unless otherwise stated:water samples I ug/L;vapor samples 4.5 ug/L;solid and sludge samples 5 ug/kg;wipes 0.2ug/wipe <br />' ND means not detected above the reporting limit;NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone; (c) (2-chloroethoxy) ethene; (d) 2-hexanone; (e) dichloromethane; (t) 2-butanone; (g) 4-methyl-2- <br /> pentanone or isopropylacetone; (h)lighter than water immiscible sheen is present, (i) liquid sample that contains greater than —5 vol. % <br /> sediment; 0) sample diluted due to high organic content; (k) ethenylbenzene; (1) methylbenzene; (m) acetic acid ethenyl ester; (n) <br /> chloroethene;(o)dimethylbenzenes. <br /> DHS Certification No. 1644 Edward Hamilton, Lab Director <br />