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Lancaster <br /> Laboratories Analysis Report <br /> 2425 New Holland Pike,PO Box 12425,Lancaster,PA 176052425•717-656-2300 Fan:717-65E2681•www.lamasteriabs.com <br /> Page I of 2 <br /> Lancaster Laboratories Sample No. SW 4186764 <br /> PL3-5' Soil Sample <br /> Facility: CPL Tracy KLM 151.1 <br /> Tracy KLM 151.5 <br /> Collected:12/15/2003 10:50 by AS Account Number: 11454 <br /> Submitted: 12/17/2003 09:25 ChevronTexaco C/o Cambria Env. <br /> Reported: 12/24/2003 at 16:49 4111 Citrus Avenue <br /> Discard: 01/24/2004 Suite 9 <br /> Rocklin CA 95677 <br /> KLMP3 <br /> As Received <br /> CAT As Received Method Dilution <br /> No. Analysis Name CAS Number Result Detection Units Factor <br /> Limit <br /> 02729 Custom TPH with Ranges (soil) <br /> 02730 Total TPH n.a. 21,000. 400. mg/kg 10 <br /> 06086 C13 - C40 n.a. 21,000. 400. mg/kg 10 <br /> Site-specific MS/MSD samples were not submitted for the project. A LCS/LCSD <br /> was performed to demonstrate precision and accuracy at a batch level. <br /> Due to the nature of the sample extract matrix, the normal final volume could <br /> not be attained. The reporting limits were raised accordingly. <br /> Accurate surrogate recoveries could not be determined due to the dilution <br /> required for analysis of the sample. <br /> 05550 TPH-GAO CA LUFT (Soils) <br /> 05555 TPH - GRO CA LUFT (Soils) n.a. 3,900. 80. mg/kg 10000 <br /> The analysis for volatiles was performed on a sample which was preserved <br /> in methanol. The reporting limits were adjusted appropriately. <br /> A poor surrogate recovery was observed due to the dilution needed to <br /> perform the analysis. <br /> 05878 BTEX <br /> 02174 Benzene 71-43-2 N.D. 50. mg/kg 10000 <br /> 02177 Toluene 108-80-3 75. 2.0 <br /> mg/kg 10000 <br /> 02178 Ethylbenzene 100-41-4 22. 2.0 mg/kg 10000 <br /> 02182 Total Xylenes 1330-20-7 130. 6.0 mg/kg 10000 <br /> The analysis for volatiles was performed on a sample which was preserved <br /> in methanol. The reporting limits were adjusted appropriately. <br /> A poor surrogate recovery was observed due to the dilution needed to <br /> perform the analysis. <br /> Due to the presence of an interferent near its retention time, the normal <br /> reporting limit was not attained for benzene. The <br /> presence or concentration of this compound cannot be determined due to the <br /> presence of this interferent. <br /> State of California Lab Certification No. 2116 <br /> Laboratory Chronicle <br />