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* SPL BATCH QUALITY CONTROL REPORT ** PAGHOUSTON LABORATORY <br /> Mod 8015 - Diesel 8880 INTERCHANGE DRIVE <br /> "O HOUSTON TEXAS 77054 <br /> PHONE(713)660.0901 <br /> Matrix Aqueous Batch Id HP_T960313030801 <br /> Units mg/L <br /> L A B O R A T 0 R Y C 0 N T R 0 L S A M F L E <br /> S P I K E Method Spike Blank Spike QC Limits(**) <br /> C O M P O U N D S Blank Result Added Result Recovery (Mandatory) <br /> c2> <3> <1> is t Recovery Range <br /> Diesel Petr Hydrocarbons ND 5 0 0 83 16 6 * 20 - 130 <br /> M A T R I X S P I K E S <br /> S P I K E Sample Spike Matrix Spike Matrix Spike MS/MSD QC Limits(***) <br /> C O M P O U N D S Results Added Duplicate Relative t (Advisory_ <br /> Result Recovery Result Recovery Difference RPD <br /> <2> <3> <1> <4> <1> <5> Max Recovery Range <br /> DIESEL PETR HYDROCARBONS 3 67 5 0 7 15 69 6 6 59 58 4 17 5 43 20 - 177 <br /> Analyst RR - Values Outside QC Range <br /> Sequence Date 03/13/96 NC = Not a cu a xceeds spike by factor of 4 or more) <br /> SPL ID of sample spiked 9603233-OIB NO = Not Detected/Below Detection Limit <br /> Sample File ID TT-595 TXO W Recovery = [( <1> - <2> ) / <3> 1 x 100 <br /> Method Blank File ID LCS % Recovery - (<1> / <3> y x 100 <br /> Wank Spike File ID TT 605 TXO Relative Percent Difference I (<4> - <5> / [(<4> + <5> 1 x 0 51 x 100 <br /> trix Spike File ID TT 589 TXO (**1 = Source SPL-Hous[on Historical Data (2nd Q 194) <br /> Matrix Spike Duplicate File ID TT_590 TXO (***) = Source SPL-Houston Historical Oata <br /> SAMPLES IN BATCH(SPL ID) 9603227-01B 9603232-OIB 9603233-OIB 9603227-03B <br /> 9603227-02B 9603233-02B <br /> / <br /> i <br /> QC Officer k <br /> ` J <br />