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• i( � r 1 <br /> Lancaster <br /> Laboratories Analysis Report <br /> 2425 New Holland Pike,PO Box 12425,Lancaster.PA 17605-2425•717-656-2300 Fax:717-656-2681•www.lancasterlabs.com <br /> Page 3 of 6 <br /> {� Quality Control Summary <br /> x <br /> Client Name: Secor International Group Number: 842784 <br /> Reported: 03/05/03 at 07:48 PM <br /> Sample Matrix Quality Control <br /> MS MSD MS/MSD RPD BRG DIIP DIIP Dup <br /> RPD <br /> Analysis Name %REC %REC Limits RPD MAX Conc Conc RPD Max <br /> Batch number: 030580009A Sample number(s) : 4001931 <br /> PCB-1016 86 86 41-140 1 5o <br /> PCB-1260 87 89 40-142 1 50 <br /> Batch number: 030585708001 Sample number(s) : 4001931 <br /> Cadmium 95 94 75-125 1 20 0.46 0.39 18 (1) 20 <br /> Chromium 102 107 75-125 2 20 20.8 19.5 7 (1) 20 <br /> Lead 119 69* 75-125 32* 20 31.2 22.2 34* (1) 20 <br /> Nickel 96 99 75-125 2 20 19.6 20.7 5 (1) 20 <br /> Zinc 147* 86 75-125 - 25* 20 - 63.9 60.4 6 20 <br /> Batch number: 03059A33A Sample number(s) : 4001931 <br /> TPH-GRO - Soils 99 115 70-130 15 30 <br /> Batch number: 03061042501A Sample number(s) : 4001931 <br /> Hexavalent Chromium (SOLIDS) 92 87 75-125 8 11 N.D. 2.4 159* (1) 20 <br /> Batch number: D030581AA Sample number(s) : 4001932-4001936,4001942 <br /> Methyl Tertiary Butyl Ether 86 90 57-136 3 30 <br /> di-Isopropyl ether 76 82 55-132 7 30 <br /> Ethyl t-butyl ether 83 89 58-127 7 30 <br /> t-Amyl methyl ether 86 90 58-126 4 30 <br /> t-Butyl alcohol 84 92 14-185 8 30 <br /> Benzene 84 92 52-141 8 30 <br /> Toluene 85 95 53-137 10 30 <br /> Ethylbenzene 83 92 50-136 10 30 <br /> Xylene (Total) 84 93 47-139. 9 30 <br /> Batch number: K030572AB Sample number(s) : 4001937-4001938,4001940 <br /> Methyl Tertiary Butyl Ether 88 86 57-136 2 30 <br /> di-Isopropyl ether 99 96 55-132 2 30 <br /> Ethyl t-butyl ether 101 98 58-127 2 30 <br /> t-Amyl methyl ether 95 94 58-126 0 30 <br /> t-Butyl alcohol 54 54 14-185 1 30 <br /> Benzene 107 98 52-141 8 30 <br /> Toluene 98 94 53-137 4 30 <br /> Ethylbenzene 106 99 50-136 7 30 <br /> Xylene (Total) 108 100 47-139 6 30 <br /> Batch number: K030572AC Sample number(s) : 4001931,4001937,4001939,4001941 <br /> Methyl Tertiary Butyl Ether 88 86 57-136 2 30 <br /> di-Isopropyl ether 99 96 55-132 2 30 <br /> Ethyl t-butyl ether 101 98 58-127 2 30 <br /> t-Amyl methyl ether 95 94 58-126 0 30 <br /> t-Butyl alcohol 54 54 14-185 1 30 <br /> Chloromethane 104 89 28-151 16 30 <br /> vinyl Chloride 117 97 33-147 19 30 <br /> Bromomethane 102 87 25-148 16 30 <br /> Chloroethane 107 91 33-147 16 30 <br /> Trichlorofluoromethane 119 104 26-157 13 30 <br /> 1,1-Dichloroethene 109 101 48-147 7 30 <br /> Methylene Chloride 97 92 59-135 5 30 <br /> trans-1,2-Dichloroethene .105 98 52-136 6 30 <br /> 1,1-Dichloroethane 105 102 60-133 3 30 <br /> cis-1,2-Dichloroethene 104 99 59-130 4 30 <br /> *-Outside of specification <br /> (1) The result for one or both determinations was less than five times the LOQ. <br /> (2) The background result was more than four times the spike added. <br /> r,, <br />