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401Lancaster Anal sis Report . Laboratories Y 2425 New Holland Pike PO Box 12425 Lancaster PA 1760,5-242 5•717-656-2300 Fax 717-656.2681•www lancasterlabs.com Page 6 of 7 Quality Control Summary Client Name ChevronTexaco Group Number 931884 Reported 02/25/05 at 10 34 AM Surrogate Quality Control 4465285 110 4465286 108 4465287 105 4465288 104 Blank 103 LCS 105 MS 108 MSD 108 Limits 80-132 Analysis Name BTEX+MTBE by 82608 Batch number Z050492AA4-Bromofluorobenzene Dibromofluoromethane 1,2-Dichloroethane-d4 Toluene-dB 87 4465277 101 94 103 89 Blank 99 91 101 93 LCS 99 92 101 94 MS 100 45 g4 MSD 101 94 101 Limats 81-120 B2-112 85-112 83-113 alysis Name BTEX+5 oxygenates+EDC+EDB+ETOH tch number Z050531AA4-d4 Dibromofluoromethane 1,2-Di chloroethane-d4 Toluene-d8 90 4465279 90 90 92 90 4465280 90 90 92 92 4465281 90 90 91 90 4465282 90 90 92 90 4455283 90 89 90 4465284 90 90 9z 9393 4465285 89 87 92 91 4465286 89 S7 92 91 Blank 90 90 92 92 LCS 90 90 92 91 MS 91 90 92 92 MSD 90 Limits 81-120 82-112 85-112 83-113 Analysis Name BTEX+5 0xygenates+EDC+EDB+ET0H Batch number Z050532AA4-Bromofluorobenzene Dibromofluoromethane 1,2-Dxchloroethane-d4 Toluene-ds 92 4465278 96 95 96 9191 Blank 93 96 96 93 LCS 94 92 94 95 MS 94 98 95 95 MSD 95 Limits 81-120 82-112 55-112 83-313 Analysis Name BTEX+5 oxygenates+EDC+EDB+ETDH Batch number Z050533AA4-Bromofluorobenzene Dibromofluoromethane 1,2-Dichloroethane-d4 Toluene-d8 "-Outside of specification (1) The result for one or both determinations was less than five times the LOQ The background result was more than four times the spike added