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Lancaster <br /> . Laboratories Analysis Report <br /> 2425 New Holland Pike PO Box 12425 Lancaster PA 17605-2425•717 658-2300 Fax 717-6562681•www lancasterlabs Com <br /> Page 5 of 5 <br /> Quality Control Summary <br /> Client Name C1levronTexaco Group Number: 920805 <br /> Reported 11/26/04 at 02 04 PM <br /> Surrogate Quality Control <br /> LCS 104 <br /> MS 102 <br /> MSD 104 <br /> Limits 80-132 <br /> Analysis Name BTEX+S Oxygenates+EDC+EDB+ETON <br /> Batch number Z043271AA <br /> Dibromofluoromethane 1,2-D3chloroethane-d4 Toluene-de 4-Bromofluorobenzene <br /> 4405327 98 93 99 94 <br /> 4405328 99 93 100 94 <br /> 4405329 100 94 300 94 <br /> 4405330 100 94 100 94 <br /> 4405331 99 94 99 96 <br /> 4405332 100 94 99 93 <br /> 4405333 101 95 100 93 <br /> Blank 95 92 100 96 <br /> LCS 95 94 101 98 <br /> MS 99 96 100 100 <br /> MSD 98 96 100 99 <br /> Limits 81-120 82-112 85-112 83-113 <br /> Analysis Name BTEX+5 Oxygenates+EDC+EDB+ETOH �S <br /> Batch number 7043281AA <br /> Dibromofluoromethane 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofiuorobenzene <br /> 4405334 101 95 99 94 <br /> 4405335 99 95 99 98 <br /> 4405336 9a 93 99 97 <br /> 4405337 100 95 99 95 <br /> 4405338 101 96 100 95 <br /> Blank 98 94 100 94 <br /> LCS 98 94 100 98 <br /> MS 101 95 100 97 <br /> MSD 101 95 100 98 <br /> Limits 81-120 82-112 85-112 83-113 <br /> Analysis Name 8260 Master scan (water) <br /> Batch number Z043282AA <br /> Dibromofluoromethane 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene <br /> Blank 98 94 99 96 <br /> LCS 98 95 99 96 <br /> Ms 103 95 100 99 <br /> MSD 103 97 100 100 <br /> Limits 81-120 82-112 85-112 93-113 <br /> *-Outside of specification <br /> (1) The result for one or both determinations was less than five times the LOQ <br /> (2) The background result was more than four times the spike added <br />