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Lancaster <br /> Laboratories Analysis Report <br /> 2425 New Holland Pike.PO Box 12425,Lancaster,PA 17605-2425-717-656-2300 Fax:717-656-2681•WWW,IaMasteriabs.0om <br /> Pagel of 2 <br /> Lancaster Laboratories Sample No. SW 4249191 <br /> MW-14-S-24-040331 Crab Soil <br /> Facility# 90557 STRC <br /> 139 S Center St Stockton T0607700391 MW-14 <br /> Collected:03/31/2004 09:33 by BM Account Number: 10869 <br /> Submitted: 04/06/2004 09 : 00 ChevronTexaco <br /> Reported: 04/15/2004 at 17: 13 6001 Bollinger Canyon Rd L4310 <br /> Discard: 05/16/2004 San Ramon CA 94583 <br /> 1424- <br /> As Received <br /> CAT As Received Method Dilution <br /> No. Analysis Name CAS Number Result Detection Units Factor <br /> Limit <br /> 01725 TPH-GRO - Soils n.a. N.D. 1.0 mg/kg 25 <br /> The analysis for volatiles was performed on a sample which was preserved <br /> in methanol. The reporting limits were adjusted appropriately. <br /> The reported concentration of TPH-GRO does not include MTBE or other <br /> gasoline constituents eluting prior to the C6 (n-hexane) TPH-GRO range <br /> start time. <br /> 05547 TPH - DRO CA LUFT (Soils) n.a, N.D. 10. mg/kg 1 <br /> According to the California LUFT Protocol, the quantitation for Diesel <br /> Range Organics was performed by peak area comparison of the sample pattern <br /> to that of our #2 fuel oil reference standard (between CIO and C28 normal <br /> hydrocarbons) . <br /> 02516 TPH Fuels by GC (Soils) <br /> 02518 Total TPH n.a. N.D. 10. mg/kg 1 <br /> 02552 TPH Motor Oil C16-C36 n.a. N.D. 10. mg/kg 1 <br /> TPH quantitation is based on peak area comparison of the sample pattern to <br /> that of a hydrocarbon component mix calibration in a range that includes <br /> C8 (n-octane) through C40 (n-tetracontane) normal hydrocarbons. <br /> The chlorobenzene surrogate recovery in the associated method blank is above the <br /> QC limit. Since the recovery is high and no target analytes are detected in the <br /> method blank, the sample results are reported. <br /> 07361 BTEX+5 Oxygenates+EDC+EDB <br /> 02016 Methyl Tertiary Butyl Ether 1634-04-4 N.D. 0.0005 mg/kg 0.99 <br /> 02017 di-Isopropyl ether IOB-20-3 N,D. 0.001 mg/kg 0.99 <br /> 02018 Ethyl t-butyl ether 637-92-3 N.D. 0.001 mg/kg 0.99 <br /> 02019 t-Amyl methyl. ether 994-05-8 N.D. 0.001 mg/kg 0.99 <br /> 02020 t-Butyl alcohol 75-65-0 N.1). 0.020 mg/kg 0.99 <br /> 05460 Benzene 71-43-2 N.D. 0.0005 mg/kg 0.99 <br /> 05461 1,2-Dichloroethane 107-06-2 N.D. 0.001 mg/kg 0.99 <br /> 05466 Toluene 108-88-3 N.D. 0.001 mg/kg 0.99 <br /> 05471 1,2-Dibromoethane 106-93-4 N.D. 0.001 mg/kg 0.99 <br /> 05474 Ethylbenzene 300-41-4 N.D. 0.001 mg/kg 0.99 <br /> 06301 Xylene (Total) 3330-20-7 N.D. 0.001 mg/kg 0.99 <br /> State of California Lab Certification No. 2116 <br /> Laboratory Chronicle <br />