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I <br /> Lancaster Laboratories <br /> Where quality is a science. <br /> I <br /> Page I of 2 <br /> ILancaster Laboratories Sample No. WW 3788172 <br /> Collected: 03/12/2002 11 :45 by SC Account Number: 10869 <br /> ISubmitted: 03/14/2002 09:20 Chevron Products Company <br /> Reported: 03/27/2002 at 15:02 6001 Bollinger Canyon Rd <br /> I Discard: 04/27/2002 Building L, PO Box 6004 <br /> MW-9S-W-020312 Grab Water San Ramon CA 94583-0904 <br /> Facility# 90557 SIRC <br /> I139 S. Center St Stockton T0607-700391 MW-9S <br /> 9SSCS <br /> I A3 Received <br /> CAT As Received Method Dilution <br /> No. Analysis Name CAS Number Result Detection Units Factor <br /> Limit <br /> 01?28 TPH-GRO - Waters n.a. 200,000. 13,000. ug/1 250 <br /> The reported concentration of TPH-GAO does not include MTBE or other <br /> gasoline constituents eluting prior to the C6 (n-hexane) TPH-GRO range <br /> start time. <br /> 5553 TPH - DRO CA LUFT (Waters) n.a. 19,000. 1,900. ug/1 100 <br /> According to the California LUFT Protocol, the quantitation for Diesel <br /> Range organics was performed by peak area comparison of the sample pattern <br /> to that of our 02 fuel oil reference standard (between C10 and C28 normal <br /> I hydrocarbons) . <br /> Site-specific MS/MSD samples were not submitted for the project. A LCS/LCSD <br /> was performed to demonstrate precision and accuracy at a batch level.. <br /> The observed sample pattern is not typical of diesel/#2 fuel oil. <br /> 01412 Methanol and Ethanol <br /> 01414 Methanol (by Direct Injection) 67-56-1 290. 200. ug/1 1 <br /> 02500 TPH Fuels by GC (Waters) <br /> I 02501 Total TPH n.a. 2,300. 1,000. ug/l 1 <br /> 02508 TPH Motor Oil C16-C36 n.a. 2,300. 1,000. ug/1 1 <br /> TPH quantitation is based on peak area comparison of the sample pattern to <br /> that of a hydrocarbon component mix calibration in a range that includes <br /> C8 (n-octane) through C40 (n-tetracontane) normal hydrocarbons. <br /> Site-specific MS/MSD samples were not submitted for the project. A LCS/LCSD <br /> was performed to demonstrate precision and accuracy at a batch level. <br /> I 01594 BTEH + Oxygenates by 8260B <br /> 01587 Ethanol 64-17-5 N.D. 5,000. ug/l 100 <br /> 02010 Methyl t-butyl ether 1634-04-4 N.D. 50. ug/1 100 <br /> I 02011 di-Isopropyl ether 108-20-3 N.D. 50. ug/l 100 <br /> 02013 Ethyl t-butyl ether 637-92-3 N.D. 50. ug/1 100 <br /> 02014 t-Amyl methyl ether 994-05-8 N.D. 50. ug/1 100 <br /> 2015 t-Butyl alcohol 75-65-0 N.D. 500. ug/1 100 <br /> I <br /> Lancaster Laboratories,Inc. <br /> I M 2425 New Holland Pike <br /> PQ Bar 12425 <br /> Lancaster,PA 17605-2425 <br /> 717-656-2300 Fax: 717-656-2691 2216 Rev.9/11100 <br />