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s 4 <br /> Lancaster Laboratories Page 3 of <br /> Where quality is a science. <br /> Quality Control Summary <br /> Ciient Dame: Chevron Products Company Group Numbcr: 804467 <br /> Reported: 05/01/02 at 12:26 PM <br /> Sample Matrix Quality Control <br /> Ms MSD M3/MSD RM EKG DUP DUP Dup <br /> RPD <br /> Analysis Name %TIBC %REC Limits RPD MAX Conc Conc RPD Max <br /> Batch number: 02109A16A Sample number(s} : 3807003--3807005 <br /> Benzene 116 77-131 <br /> Toluene 116 80-128 <br /> Ethylbenzene lil 76-132 <br /> Total Xylenes 111 76-132 <br /> Methyl tert-Butyl Ether 95 61-144 <br /> TPH-GRO - Waters 106 74-132 <br /> Batch number: 021120028A Sample number(s) : 3807003-3807013 <br /> Methanol (by Direct Injection) 84 88 58-137 5 20 <br /> Batch number: 021150021A Sample number(s) : 3807014-3807015 <br /> Methanol (by Direct Injection) 76 76 58-137 0 20 <br /> Batch number: V021071AB Sample number(s) : 3807004-3807010,3807014-3807015 <br /> Ethanol 84 93 70-130 10 30 <br /> Methyl t-butyl ether 105 104 69-134 1 30 <br /> di-Isopropyl ether 107 106 68-133 1 30 <br /> Ethyl t-butyl ether 106 104 73-123 2 30 <br /> t-Amyl methyl ether 107 103 69-118 4 30 <br /> t-Butyl alcohol 115 109 51-148 5 30 <br /> ,2-Dichloroethane 102 110 75-141 7 30 <br /> 2-Dibromoethane 106 102 78-120 4 30 <br /> Batch number: V021091AB Sample number(s) : 3807003,3807011-3B07013 <br /> Ethanol 101 92 70-130 9 30 <br /> Methyl t-butyl ether 102 102 69-134 0 30 <br /> di-Isopropyl ether 110 110 68-133 0 30 <br /> Ethyl t-butyl ether 106 107 73-123 0 30 <br /> t-Amyl methyl ether 105 105 69-118 0 30 <br /> t-Butyl alcohol 102 98 51-148 4 30 <br /> 1,2-Dichloroethane 115 116 75-141 0 30 <br /> 1,2-Dibromoethane 101 99 78-120 2 30 <br /> Surrogate Quality Control <br /> Analysis Name: TPH Fuels by GC (Waters) <br /> Batch number: 021080014A J109 <br /> Orthoterphenyl <br /> 3807003 80 <br /> 3807004 80 <br /> 3807005 81 <br /> 3807006 81 <br /> 3807007 79 <br /> 3807008 79 <br /> 3807009 64 <br /> 3807010 78 <br /> *-Outside of specification <br /> l) The result for one or both determinations was less than five times the LOQ. <br /> The background result was more than four times the spike added. <br /> Lancaster Laboratories,Inc. <br /> MEMBER 2425 New Holland Pike <br /> ® PO Box 12425 <br /> Lancaster,PA 17605-2425 <br /> 717-656-2300 Fax:717-656-2681 2216 Rev.9/11/00 <br />