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h <br /> Analysis Report <br /> Lancaster <br /> i Laboratories <br /> Page 5 of 7 <br /> Quality Control Summary <br /> Client Name: Secor International Group Number: 842784 <br /> Reported: 03/05/03 at 07 :48 PM <br /> Sample Matrix Quality Control. <br /> MS MSD MS/MSD RPD EKG DUP DUP Dup <br /> RPD <br /> Analysis Name %REC %REC Limits RPD MAX Conc Conc RPD Max <br /> Dibromochloromethane 90 89 53-130 1 30 <br /> Chlorobenzene 101 97 59-125 4 30 <br /> Ethylbenzene 106 99 50-136 7 30 <br /> m+p-Xylene 108 101 47-139 6 30 <br /> o-Xylene 107 99 47-139 7 30 <br /> Bromoform 77 75 46-128 3 30 <br /> 1,1,2,2-Tetrachloroethane 72 72 31-166 0 30 <br /> 1,3-Dichlorobenzene 100 91 51-134 9 30 <br /> 1,4-Dichlorobenzene 100 91 52-132 8 30 <br /> 1,2-Dichlorobenzene 97 89 51-133 8 30 <br /> trans-1,3-Dichloropropene 87 86 51-127 0 30 <br /> cis-1,3-Dichloropropene 100 94 50-129 5 30 <br /> Xylene (Total) 108 100 47-139 6 30 <br /> Freon 113 110 101 39-146 8 30 <br /> 0 Surrogate Quality Control <br /> Analysis Name: TPH-GRD - Soils <br /> Batch number: 03057A31B <br /> Trifluorotoluene-F <br /> 4001932 82 <br /> 4001933 80 <br /> 4001934 82 <br /> 4001935 82 <br /> 4001936 87 <br /> 4001937 87 <br /> Blank 97 <br /> LCS 110 <br /> MS 90 <br /> MSD 83 <br /> Limits: 66-117 <br /> Analysis Name: TPH-GRO - Soils <br /> Batch number: 03057A34B <br /> Trifluorotoluene-F <br /> 4001938 81 <br /> 4001939 84 <br /> 4001940 90 <br /> *-Outside of specification <br /> (1) The result for one or both determinations was less than five times the LOQ. <br /> The background result was more than four times the spike added. <br /> Lancaster Laboratories,Inc. <br /> MEMBER 2425 New Holland Pike <br /> PO Box 12425 <br /> Lancaster, 17605 2425 <br /> 717-656-230000 Fa x:717-656-2681 2216 Rev.10/2102 <br />