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Lancaster <br /> • Laboratories <br /> Page 7 of 7 <br /> Quality Control Summary <br /> Client Name: Secor International Group Number: 842784 <br /> Reported: 03/05/03 at 07 :48 PM <br /> Surrogate Quality Control <br /> 4001932 95 89 94 87 <br /> 4001933 96 88 96 87 <br /> 4001934 96 92 94 88 <br /> 4001935 97 89 95 87 <br /> 4001936 95 89 93 86 <br /> 4001942 100 88 113 69* <br /> Blank 93 93 92 90 <br /> LCS 94 92 94 89 <br /> MS 92 92 96 89 <br /> MSD 94 91 97 88 <br /> Limits: 80-120 80-120 81-117 74-121 <br /> Analysis Name: PPL + xylene (total) by 8260 <br /> Batch number: K030572AS <br /> Dibromofluoromethane 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene <br /> 4001937 95 80 94 87 <br /> 4001938 97 85 104 83 <br /> WS1940 97 83 97 86 <br /> nk 99 91 96 90 <br /> 99 88 102 96 <br /> MS 96 87 103 95 <br /> MSD 96 88 101 95 <br /> Limits: 80-120 80-120 81-117 74-121 <br /> Analysis Name: PPL + Xylene (total) by 8260 <br /> Batch number: K030572AC <br /> Dibromofluoromethane 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene <br /> 4001931 96 83 99 92 <br /> 4001939 98 85 98 79 <br /> 4001941 97 84 102 84 <br /> Blank 94 87 97 93 <br /> LCS 99 88 102 96 <br /> MS 96 87 103 95 <br /> MSD 96 88 101 95 <br /> Limits: 80-120 80-120 81-117 74-121 <br /> *-Outside of specification <br /> (1) The result for one or both determinations was less than five times the LOQ. <br /> The background result was more than four times the spike added. <br /> Lancaster Laboratories,Inc. <br /> M E M S I— R 2425 New Holland Pike <br /> PO Box 12425 <br /> ® Lancaster, 17605-2425 <br /> 717-656-230000 Fax:717-656-2681 2216 Rev.1012l02 <br />