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METHOD SN503•260B • VOLATILE ORGANICS BY GC/MS - Client : HALEY & ALDRICH, INC. Date Collected: 05/07/15 Project : ABB STOCKTON Date Received: 05/08/15 Batch No : 15EO45 Date Extracted. 05/11/15 16:53 Sample ID: SB-11.-2.5-3.0 Date Analyzed: 05//11/15 16:53 Lab Samp ID- E045.07 Dilution Factor: 1.D6 Lab FileID: REP129 Matrix : SOIL Ext Btch ID: VS02EO7 % Moisture : 21.2 Calib. Ref.; RDPO51 Instrument ID : T-002 ESULS RL PARAMETERS (ug/kg) (ug/kg) (ug/kg ---------- ------- ------- ------- 1,1,1,2-TETRACHLOROETHANE ND 6.7 1.3 1 1,1-TRICHLOROETHANE ND 6.7 1.3 1;1,2,2-TETRACHLOROETHANE ND 6.7 1.3 1,1,2-TRICHLOROETHANE ND 6.77 3 1,1-DICHLOROETHANE ND 6.7 1.3 1,1-DICHLOROETHENE ND 6.7 1.3 1,1-DICHLOROPROPENE ND 6.7 1.3 1,2,3-TR ICHLDROBENZENE NO g.7 2.7 1,213-TRICHLOROPROPANE NO 2.7 1,2,44-TRICHLOROBENZENE ND bg 2.7 1,2,4-TRIMETHYLBENZENE ND 6. 2.7 1,2-DISROMO.3-CHLOROPROPANE NO 6.7 2. 1,2-DIBROMOETHANE ND 6.7 1.3 1 2-DICHLOROBENZENE ND 6.7 1.3 1;2-OICHLOROETHANE ND bb 7 1.3 1,2-DICHLOROPROPANE NO 6.7 1 .3 1,3,5-TRIMETHYLBENZENE NO 6g 7 2.7 1,3-DICHLOROBENZENE NO 6.7 1.3 1,3-DICHLOROPROPANE NO 6.7 1.3 1,4-DICHLOROBENZENE NO 6.7 1.3 2,2-DICHLOROPROPANE ND 6.7 2.7 2-BUTANONE (MEK) NO 13 6.7 2-CHLOROTOLUENE ND 6.7 1.3 2-HEXANONE NO 13 6.7 4-CHLOROTOLUENE NO 6.7 1.3 BENZENE. 2631 617 11.3 BROMOBENZENE ND 6.7 1.3 BROMOCHLOROMETHANE NO 6.7 1.3 - BROMODICHLOROMETHANE ND 6.7 1.3 BROMOFORM ND 6.7 2.7 BROMDMCARBONDISULFIDEND 6THANE ND 1 ON7 1.3 CARBON TETRACHLORIDE ND 6.7 1.3 CHLOROBENZENE ND 6.7 1.3 CHLOROETHANE ND 6.7 2.7 CHLOROFORM ND7 1.3 CHLOROMETHANE ND .7 2.7 CIS-1,2ND 6.7 1.3 CIS-1 3-DICHLOROPROPENE ND 6.7 1.3 DIBRONOCHLOROMETHANE ND 6.7 1.3 DIBROMOMETHANE NO 6.7 1.3 DICHLORODIFLUOROMETHANE ND 6.7 2.7 ETHYLBENZENE ND 6.7 1.3 HEXACHLOROBUTADIENE ND 6.7 2.7 ISOPROPYL BENZENE NO 6.7 2.7 M,P-XYLENES NO 13 2.7 4-METHYL-2-PENTANONE (MIRK) NO 13 6.7 METHYLENE CHLORIDE NO 13 2.7 METHYL-TERT-BUTYL ETHER (MTBE) NO 6.7 1.3 NAPHTHALENE ND 13 2.7 N-BUTYLBENZENE NO 6.7 1.3 N-PROPYLBENZENE ND 6.7 1.3 O-XYLENE NO 6.7 1.3 P-ISOPROPYLTOLUENE NO 6.7 1.3 SEC-BUTYLBENZENE NO 6.7 1.3 STYRENE ND 6.7 1.3 TERT-BUTYLBENZENE NO 6.7 1.3 TETRACHLOROETHENE NO 6.7 1.3 TOLUENE ND 6.7 1.3 TRANS-I,2-DICHLOROETHENE ND 6.7 1.3 TRANS-1 3-DICHLOROPROPENE NO 6.7 1.3 TRICHLOAlOETHENE NO 6.7 1.3 TRICHLOROFLUOROMETHANE ND 6.7 2.7 VINYL CHLORIDE ND 6.7 2.7 SURROGATE PARAMETERS RESULTS SPK AMT % RECOVERY OC LIMIT -------------------- ------- ...--- ---------- -------- 1,2-DICHLOROETHANE-D4 71.3 67.26 106 60-160 4-BROMOFLUOROBENZENE 73 9 67.26 110 85-120 TOLUENE-D8 72.3 67.26 108 85-115 DISROMOFLUOROMETHANE 71.5 67.26 106 70-130 °?CA 5 f35