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METHOD SW3550B/8270C • <br /> SEMI VOLATILE ORGANICS BY GC/MS <br /> Client HALEY & ALDRICH, INC. Date Collected 05/07/15 <br /> Project ASB STOCKTON Date Received 05/08/15 <br /> Batch No 15EO45 Date Extracted 05/11/15 11.45. <br /> Sample ID. SB-08-1.5-2.0 Date Analyzed. 05/11/15 19:06 <br /> Lab-Samp ID: E045-04 Dilution Factor: 1 <br /> Lab File ID: REJ136 - Matrix SOIL <br /> ExtBtch ID: SVE006S Z Moisture 16.7 <br /> Calib. Ref.: RLJO13 Instrument ID T-OE4 <br /> RESULTS RL MDL <br /> PARAMETERS (ug/kg) (ug/kg) (ug/kg) <br /> __--______ <br /> 1,2,4-TRICHLOROBENZENE NO 400 200 <br /> 1,2-DICHLOROSENZENE NO 400 200 <br /> 1,2-DIPHENYLHYORAZINE (3) NO 400 200 <br /> 1,3-DICHLOROBENZENE NO 400 200 <br /> 1,4-DICHLOROBENZENE NO 400 200 <br /> 2,4,5-TRICHLOROPHENOL NO 400 200 <br /> 2,4,6-TRICHLOROPHENOL NO 400 200 <br /> 2,4-DICHLOROPHENOL ND 400 200 <br /> 214-DIMETHYLPHENOL ND 400 200 <br /> 2,4-DINITROPHENOL NO 800 200 <br /> 2,4-DINITROTOLUENE NO 400 200 <br /> 2,6-OINITROTOLUENE NO 400 200 <br /> 2-CHLORONAPHTHALENE ND 400 200 <br /> 2-CHLOROPHENOL NO 400 200 <br /> 2-METHYLNAPHTHALENE ND 400 200 <br /> 2-METHYLPHENOL ND 400 200 <br /> 2-NITROANILINE NO 400 200 <br /> 2-NITROPHENOL NO 400 200 <br /> 3,31-DICHLOROBENZIDINE NO 400 200 <br /> 4-METHYLPHENOL (1) ND 400 200 <br /> 3-NITROANILINE ND 400 200 <br /> 4,6-DINITRO-2-METHYLPHENOL ND 800 200 <br /> 4-BROMOPHENYL-PHENYL ETHER ND 400 200 <br /> 4-CHLORO-3-METHYLPHENOL ND 400 200 <br /> 4-CHLOROANILINE ND 400 200 <br /> 4-CHLOROPHENYL-PHENYL ETHER ND 400 200 - <br /> 4-NITROANILINE ND 400 200 <br /> 4-NITROPHENOL ND 800 200 <br /> ACENAPHTHENE ND 400 200 <br /> ACENAPHTHYLENE 3901 400 200 <br /> ANTHRACENE 250J 400 200 <br /> BENZO(A)ANTHRACENE 910 400 200 <br /> BENZO(A)PYRENE 2300 400 200 <br /> BENZO(8)FLUORANTHENE 2100 400 200 <br /> BENZO(G H I)PERYLENE 2400 400 200 <br /> BENZO(KSFCUORANTHENE 510 400 200 <br /> BENZOIC ACID ND 1600 800 <br /> BENZYL ALCOHOL ND 400 200 <br /> 8IS(2-CHLOROISOPROPYL)ETHER ND 400 200 <br /> BIS(2-CHLOROETHOXY)METHANE ND 400 200 <br /> BIS(2-CHLOROETHYL)ETHER ND 400 200 <br /> BIS(2-ETHYLHEXYL)PHTHALATE NO 400 200 <br /> BUTYLBENZYLPHTHALATE NO 400 200 <br /> CARBAZOLE NO 400 200 <br /> CHRYSENE 1200 400 200 <br /> DISENZO(A H)ANTHRACENE ND 400 200 <br /> DISENZOFUkAN ND 400 200 <br /> DIETHYLPHTHALATE NO 400 200 <br /> DIMETHYLPHTHALATE NO 400 200 <br /> DI-N`BUTYLPHTHALATE NO 400 200 <br /> DI-N-OCTYLPHTHALATE ND 400 200 <br /> FLUORANTHENE 3500 400 200 <br /> 400 200 <br /> FLUORENE ND <br /> HEXACHLOROSENZENE NO 400 200 <br /> HEXACHLOROBUTADIENE NO 400 200 <br /> HEXACHLOROETHANE NO 400 200 <br /> INDENO(1 2,3-CD)PYRENE 1500 400 200 <br /> ISOPHOROAIE ND 400 200 <br /> NAPHTHALENE 220J 400 200 <br /> NITROBENZENE ND 400 200 <br /> N-NITROSODIMETHYLAMINE NO 400 200 <br /> N-NITROSO-DI-N-PROPYLAMINE ND 400 200 <br /> N-N I TROSODIPHENYLAMINE (2) ND 400 200 <br /> PENTACHLOROPHENOL ND 800 200 <br /> PHENANTHRENE 2300 400 200 <br /> PHENOLND 400 200 <br /> PYRENE 4000 400 200 <br /> SURROGATE PARAMETERS RESULTS SPK AMT Y. RECOVERY OC LIMIT <br /> -------------------- ------- ___v___ __________ <br /> 2,4 6-TRIBROMOPHENOL 1470 2401 61.1 35-125 <br /> 2-FCUOROBIPHENYL 484 800.4 60.5 45-105 <br /> 2-FLUOROPHENOL 1210 2401 50.5 35-105 <br /> NITROBENZENE-D5 468 800.4 58.5 35-100 <br /> PHENOL-D5 1350 2401 56.4 40-100 <br /> TERPHENYL-D14 532 800.4 66.5 30-125 <br /> (1):. Cannot be separated from 3-Methylphenol <br /> (2 : Cannot be separated from Diphenylamine <br /> (3): 1,2 Diphenylhydrazine analyzed as Azobenzene due to decomposition in injector <br />