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METHOD SN35506/8270C • <br /> SEMI VOLATILE ORGANICS BY GC/MS <br /> Client : HALEY 8 ALDRICH, INC. Date Collected 05/06/15 <br /> Project : ABB STOCKTON Date Received 05/07/15 <br /> Batch No. : 15EO22 Date Extracted 05/11/15 11:45 <br /> Sample ID: GB-01-0.5-1.0 Date Analyzed: 05/11/15 17:09 <br /> LabSoID: E022-.05 Dilution Factor: 1 <br /> Lab File ID: REJ130 Matrix : SOIL <br /> Ext Btch ID: SVE006S % Moisture : 11.2 <br /> Calib. Ref.: RLJO13 Instrument ID t T-OE4 <br /> RESULTS RL MDL <br /> PARAMETERS (ug/kg) (ug/kg) (ug/kg) <br /> _------ _______ _______ ....... <br /> 1,2,4-TRICHLOROBENZENE NO 370 190 <br /> 1,Z-DICHLOROBENZENE NO 370 190 <br /> 1,2-DIPHENYLHYDRAZINE (3) NO 370 190 <br /> 1,3-DICHLOROBENZENE NO 370 190 <br /> 1,4-DICHLOROBENZENE NO 370 190 <br /> 2,4,5-TRICHLOROPHENOL NO 370 190 <br /> 2,4,6-TRICHLOROPHENOL NO 370 190 <br /> 2,4-DICHLOROPHENOL ND 370 190 <br /> 2,4-DIMETHYLPHENOL ND 370 190 <br /> 2,4-DINITROPHENOL NO 750 190 <br /> 2,4-DINITROTOLUENE ND 370 190 <br /> 2,6-DINITROTOLUENE ND 370 190 <br /> 2-CHLORONAPHTHALENE ND 370 190 <br /> 2-CHLOROPHENOL ND 370 190 <br /> 2-METHYLNAPHTHALENE ND 370 190 <br /> 2-METHYLPHENOL ND 370 190 <br /> 2-NITROANILINE ND 370 190 <br /> 2-NITROPHENOL ND 370 190 <br /> 3,31-DICHLOROBENZIDINE ND 370 190 <br /> 4-METHYLPHENOL (1) ND 370 190 <br /> 3-NITROANILINE ND 370 190 <br /> 4,6-DINITRO-2-METHYLPHENOL ND 750 190 <br /> 4-BROMOPHENYL-PHENYL ETHER NO 370 190 <br /> 4-CHLORO-3-METHYLPHENOL NO 370 190 <br /> 4-CHLOROANILINE NO 370 190 <br /> 4-CHLOROPHENYL-PHENYL ETHER NO 370 190 <br /> 4-NITROANILINE NO 370 190 <br /> 4-NITROPHENOL ND 750 190 <br /> ACENAPHTHENE NO 370 190 <br /> ACENAPHTHYLENE NO 370 190 <br /> ANTHRACENE NO 370 190 <br /> 8ENZO(A)ANTHRACENE 580 370 190 <br /> BENZO(A)PYRENE 850 370 190 <br /> BENZO(8)FLUORANTHENE 980 370 190 <br /> BENZO(G H I)PERYLENE 730 370 190 <br /> BENZO(K$FCUORANTHENE 3101 370 190 <br /> BENZOIC ACID NO 1500 750 <br /> BENZYL ALCOHOL NO 370 190 <br /> BIS(2-CHLOROISOPROPYL)ETHER NO 370 190 <br /> BIS(2-CHLOROETHOXY)METHANE NO 370 190 <br /> BIS(2-CHLOROETHYL)ETHER NO 370 190 <br /> BIS(2-ETHYLHEXYL)PHTHALATE NO 370 190 <br /> BUTYLBENZYLPHTHALATE ND 370 190 <br /> CARBAZOLE ND 370 190 <br /> CHRYSENE 610 370 190 <br /> DIBENZO(A H)ANTHRACENE NO 370 190 <br /> DIBENZOFUAtAN NO 370 190 <br /> DIETHYLPHTHALATE NO 370 190 <br /> DIMETHYLPHTHALATE NO 370 190 <br /> DI-N-BUTYLPHTHALATE NO 370 190 <br /> DI-N-OCTYLPHTHALATE NO 370 190 <br /> FLUORANTHENE 1300 370 190 <br /> FLUORENE NO 370 190 <br /> HEXACHLOROBENZENE ND 370 190 <br /> HEXACHLOROBUTADIENE NO 370 190 <br /> HEXACHLOROETHANE NO 370 190 <br /> INDENO(1 2,3-CD)PYRENE 550 370 190 <br /> ISOPHOROAE ND 370 190 <br /> NAPHTHALENE NO 370 190 <br /> NITROBENZENE NO 370 190 <br /> N-NITROSODIMETHYLAMINE NO 370 190 <br /> N-NITROSO-DI-N-PROPYLAMINE ND 370 190 <br /> N-NITROSODIPHENYLAMINE (2) ND 370 190 <br /> PENTACHLOROPHENOL ND 750 190 <br /> PHENANTHRENE 720 370 190 <br /> PHENOL NO 370 190 <br /> PYRENE 1600 370 190 <br /> SURROGATE PARAMETERS RESULTS SPK AMT % RECOVERY DC LIMIT <br /> -------------------- ------- _______ ---------- -------- <br /> 2,4 6-TRIBROMOPHENOL 1400 2252 62.3 35-125 <br /> 2-FCUOROBIPHENYL 536 750.8 71.4 45-105 <br /> 2-FLUOROPHENOL 1280 2252 56.9 35-105 <br /> NITROBENZENE-D5 498 750.8 66.3 35-100 <br /> PHENOL-D5 1450 2252 64.5 40-100 <br /> TERPHENYL-D14 545 750.8 72.5 30-125 <br /> (1): Cannot be separated from 3-Methylphenol <br /> (2): Cannot be separated from Diphenylamine <br /> (3): 1,2 Diphenylhydrazine analyzed as Azobenzene due to decomposition in injector <br /> 84si A � <br />