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t <br /> 16 mm"m STL Submission# 2003-04-0616 <br /> Fuel Oxygenates by 8260B <br /> Philip Services- Illinois <br /> 1 Attn Mark Milward <br /> 210 W Sand Bank Road <br /> Colombia, IL 62236 <br />' Phone (618) 281-1547 Fax (618) 281-5120 <br /> Project 023484517 A00 Received 04/24/2003 13 40 <br /> Former Earthgrains Facility <br /> Batch QC Report <br />' Prep(s) 50308 Test(s) 8260FAB <br /> Laboratory Control Spike Water QC Batch#2003104130-01 27 <br /> LCS 2003104130-01 27-003 Extracted 04/30/2003 Analyzed 04/30/2003 10 08 <br /> LCSD 2003104130-01 27-004 Extracted 04/30/2003 Analyzed 04/30/2003 10 36 <br />' Compound Conc ug/L. Exp Conc Recovery RPD Ctrl Llmds% Flags <br /> LCS LCSD LCS LCSD % Rec RPD LCS LCSD <br /> Benzene 231 257 250 924 1028 107 69-129 20 <br /> Toluene 21 1 247 250 844 98 8 15 7 70-130 20 <br /> Methyl tert-butyl ether(MTBE) 277 293 250 1108 1172 5 6 65-165 20 <br /> Surrogates(s) <br /> 1,2-Dichloroethane-d4 497 494 500 994 988 76-114 <br /> Toluene-d8 476 489 500 952 978 88-110 <br /> 1 <br />' Severn Trent Laboratories, Inc 05/05/2003 15 48 <br /> STL San Francisco'1220 Quarry Lane Pleasanton,CA 94566 page 9 of 12 <br /> A W of Se m Tmnt Pic Tel 925 484 1919 Fax 925 484 1096"www s8-Inc Com'CA DHS EIRP#2496 <br />