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STL Submission# 2003-04-0616 <br /> 16 <br /> Fuel Oxygenates by 8260B <br /> Philip Services- Illinois <br /> Attn Mark Milward <br /> 210 W Sand Bank Road <br /> Colombia, IL 62236 <br /> ' Phone (618) 281-1547 Fax (618) 281-5120 <br /> Project C23484517 A00 Received 04/24/2003 13 40 <br /> Former Earthgrains Facility <br /> Batch QC Report <br /> IPrep(s) 5030B Test(s) 8260FAS <br /> Matrix Spike ( MS 1 MSD ) Water QC Batch#2003/05104-01 64 <br /> EFF >> MS Lab ID 2003-05-0017- 001 <br /> MS 2003105104-01 64-005 Extracted 05/05/2003 Analyzed 05/05/2003 00 13 <br /> Dilution 1 00 <br /> MSD 2003105104-01 64-006 Extracted 05/05/2003 Analyzed 05/05/2003 00 35 <br /> Dilution 1 00 <br /> Compound Conc uglL Spk Level ecove Limits% Fiags <br /> MS MSD Sample ug/L MS MSD RPD Rec RPD MS MSD <br /> ' Benzene 218 218 ND 250 872 872 0 0 69-129 20 <br /> Toluene 226 221 ND 250 904 884 2 2 70-130 20 <br /> Methyl tert-butyl ether 266 265 ND 250 1064 1060 0 4 65-165 20 <br /> Sumogafe(s) <br /> ' 1 2-Dtchloroethane-d4 542 533 500 1084 1066 76-114 0 <br /> Toluene-d8 491 491 500 982 98 2 88-110 0 <br /> 1 <br /> Sevem Trent Laboratories, Inc 05/05/2003 1548 <br /> ' STL San Francisco"1220 Quarry Lane Pleasanton CA 94566 Page 12 of 12 <br /> A pert ol5e Trent Pic Tel 925 484 1919 Fax 925 484 1096`www sti-tnc com'CA DNS FLAP#2496 <br />