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Submission 11 2002-09-0595 <br /> Fuel Oxygenates by 8260B STI <br /> Philip Services- Illinois 1122 San Francisco <br /> 220 Quarry Lane <br /> Attn Mark Mllward Pleasanton CA 94566 <br /> 210 W Sand Bank Road <br /> Colombia, IL 62236 Tel (925)484-1919 <br /> Phone (618) 281-1547 Fax (618) 281-5120 Fax (925)484-1096 <br /> www stl-inc com <br /> Project C23484517 Received 09/25/2002 18 30 www chromalab com <br /> Sara Lee (S Center St) <br /> ' CA DHS EI.AP#2496 <br /> Batch QC Report <br /> Prep(s) 5030E Test(s) 8260FAB <br /> Laboratory Control Spike Water QC Batch #2002109130-01 27 <br /> LCS 2002109130-01 27-007 Extracted 09/30/2002 Analyzed 091301200211 56 <br /> LCSD 2002109130-01 27-005 Extracted 09/30/2002 Analyzed 09/30/2002 11 12 <br /> ' <br /> Compound Conc ug/L Exp Conc Recovery RPD Ctrl Limits% Flags <br /> LCS LCSD LCS LCSD % Rec I RPD LCS LCSD <br /> Benzene 21 3 21 0 25 0 85 2 84 0 1 4 69-129 20 <br /> Toluene 236 234 250 94 4 936 0 9 70-130 20 <br /> Methyl tent-butyl ether(MTBE) 206 197 25 0 824 788 4 5 65-165 20 <br /> Surrogates(s) <br /> 1 2-Dichloroethane-d4 561 539 500 1122 1078 76-114 <br /> Toluene-d8 504 495 1500 1008 1990 88-110 <br /> 1 <br /> 1 <br /> t <br /> 10/02/2002 15 43 STL San Francisco is part of Severn Trent Laboratories Inc Page 9 of 10 <br />