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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> MCCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> http//www mccamnbell com E-mail main@mccampbell com <br /> s <br /> Advanced GeoEnvironmental Client Project ID 1=emanado's Place Date Sampled 08/17/01 <br /> 837 Shaw Road Date Received 08/21/01 <br /> Stockton, CA 95215 Client Contact Paul Dotson Date Extracted 08/21-08/22101 <br /> I Client P O Date Analyzed 08/21-08122/01 <br /> Seven Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br />' Lab ID 75277 75278 75279 75280 <br /> CPT-6/ CPT-6/ CPT-6/ CPT-6/ Reporting Limit <br /> Client 1D 18'-55' 69'-71' 88'-90' 118'-120 <br /> IMatrix W W W W S W <br /> Compound Concentration* ug/kg ug/L <br /> Di-isopropyl Ether(DIPS) ND<50 ND<50 ND<50 ND<5 0 50 10 <br /> Ethyl tert-Butyl Ether(ETRE) ND<50 ND<50 ND<50 ND<5 0 50 10 <br /> Methyl tert-Butyl Ether(MTBE) ND<50 ND<50 ND<50 ND<5 0 50 10 <br /> tent-Amyl Methyl Ether(TAME) ND<50 ND<50 ND<50 ND<5 0 50 10 <br /> tert-Butanol ND<250 ND<250 ND<250 ND<25 25 50 <br /> Methanol ND<25,000 ND<25,000 ND<25,000 ND<2500 2500 500 <br /> Ethanol ND<2500 ND<2500 ND<2500 ND<250 250 50 <br /> Surrogate Recoveries(%) <br /> IDibromofluoromethane 106 103 110 106 <br /> IComments j,h j,i j J,i <br /> "water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/STLC/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit,N/A means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present,(i)liquid sample that contains greater than—5 vol %sediment,0)sample diluted due to <br /> high organic content <br /> • <br /> I <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br /> I <br />