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I j Sequoia <br />qI&V Analytical <br />Getter Ryan, Inc - Dublin <br />6747 Sierra Court Suite J <br />Dublin CA, 94568 <br />Volat <br />Project Unocal <br />Project Number Unocal 0 0123 <br />Project Manager Deanna L Harding <br />Drganic Compounds by EPA Method 8260B <br />Sequoia Analytical - Walnut Creek <br />404 N Wlget lane <br />Walnut Credo. CA 94598 <br />(925) 988-9600 .9 <br />FAX (925) 988-9673 <br />www sequolalabs com <br />Reported: <br />29 -Dec -00 07 40 <br />Reporting <br />Analyte Result Limit Units Dilution Batch Prepared Analyzed Method Notes <br />U-7 (W0121674)7) Water <br />Sampled 06 -Dec -00 00 00 <br />Received 06 -Dec -0018:30 <br />Ethanol <br />ND <br />500 ug/1 1 OL12004 12 -Deo -00 12 -Deo -00 EPA 9260B <br />tert-Butyl alcohol <br />ND <br />50 <br />Methyl test -butyl ether <br />ND <br />20 w X w » w » <br />Dr -isopropyl ether <br />ND <br />20 » » w » w <br />Ethyl tert-butyl ether <br />ND <br />20 ^ » N N w <br />tert Amyl methyl ether <br />ND <br />20 N X N » N <br />1,2-Dichloroedme <br />ND <br />20 ^ » w w » w <br />Ethylene dribromrde <br />ND <br />20 w N N N X w <br />Surrogate Dibrornofluoromedmae <br />Surrogate 1,2 DwWroedwne-i4 <br />920% 50-150 <br />780% 50-150 ^ " <br />U-8 (W012167-08) Water Sampled 06 -Dec -00 00 00 Received 06 -Dec -N 18 30 <br />Ethanol <br />Sequoia <br />ND <br />500 ugA 1 OL12004 12-Dea-W 12 -Dao -00 EPA 8260B <br />tert-Butyl alcohol <br />ND <br />50 ^ w « » w w <br />Methyl tent -butyl ether <br />ND <br />20 X w w « n w <br />Di -isopropyl ether <br />ND <br />20 « N w w <br />• <br />Ethyl tert-butyl ether <br />ND <br />20 <br />ted-Antyl methyl ether <br />ND <br />20 w n w w w w <br />1,2 Dlchlowethane <br />ND <br />20 N » w N w w <br />Ethylene dbromlde <br />ND <br />2 0 w w w w w w <br />—Surrogate Dr brornoJluorovnethmre <br />94 0 % 50-150 <br />—Surrogate 1,-2 Drchlor�oethaned4 <br />80-0 %-50450— <br />50.150 <br />Signora Analytical - WainuE Greek The rearihaa in th}a raepWt nppiy to the aaarrplea araTyr.d in aocarxlunece with rhs chofn off <br />cu"wfy doc~mL M am dj fid reeporr nnrat be repno&ced In Ira orrd4 <br />Page 4 of 17 <br />