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, COLUMBIA ANALYTICAL SERVICES,INC <br /> QA/QC Report <br /> Client ARCO Products Compare-, Service Request. S9601408 <br /> Protect 2168 STOCKTON/217-5-234 002/TO#19350 00 Date Collected 8122196 <br /> Sample Matrix. Water Date Received 8127/96 <br /> Date Extracted NA <br /> Date Analyzed: 8130196 <br /> Matrix Spike/Duplicate Matrix Spike Summary <br /> TPH as Gasoline <br /> EP N Methods 5030/California DHS LUFT Method <br /> Units ug/L (ppb) <br /> Sample Name MW-1 (54) <br /> Lab Code 59601408-001 <br /> PerLent ReLovery <br /> CAS Relative <br /> Spike Len cl S.imple Spike Result Acceptance Percent <br /> AnalvtL MS DMS Result MS DMS MS DMS Limits DdfLrcnce <br /> Gasolinc 50000 000 i5 000 81 000 til 000 92 92 67-121 <1 <br /> Page 9 <br />