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Dave <br /> Sequoia HIM CA sol? <br /> Morgan HLA CA 95037 <br /> 1 (408)776-9600 <br /> FAX(408)782-6308 <br /> a-- Analytical wwwSequulalabscom <br /> i <br /> Blame Tech Services(Shell) Project 440 W Charter Way Sampled 11/21/00 <br /> 1680 Rogers Avenue Project Number 440 W Charter Way Received 11/22/00 <br /> San Jose,CA 95112 Project Manager Nancy Bishop Reported 1/25/0108 00 <br /> Volatile Organic Compounds by EPA Method 8260B <br /> Sequoia Analytical-Walnut Creek <br /> Batch Date Date Specific Reporting <br /> Analyte Number Prepared Analyzed Method Limit Result Units Notes* <br /> MW8 MJK0692-06 Water <br /> tert-Butyl alcohol OL05015 12/5/00 1215/00 EPA 8260E 50 ND ug/l <br /> Methyl tert-butyl ether EPA 8260B 20 ND " <br /> Di-isopropyl ether EPA 8260B 2 0 ND " <br /> Ethyl tert-butyl ether EPA 8260B 20 ND " <br /> tert-Amyl methyl ether EPA 8260B 20 ND " <br /> 1,2-Dibromoethane EPA 8260E 20 ND " <br /> 1,2-Dichloroethane EPA 8260B 2 0 ND " <br /> Surrogate Dibromofluoromethane 50-150 100 % <br /> Surrogate 1,2-D►chloroethane-d4 50-150 960 <br /> MW 10 MJK0692-07 Water <br /> tert-Butyl alcohol OL05015 12/5100 1215/00 EPA 8260B 250 ND ug/l <br /> Methyl tert-butyl ether EPA 8260B 10 ND " <br /> Di-isopropyl ether EPA 8260B 10 ND <br /> Lthyl tert-butyl ether EPA 8260B 10 ND " <br /> tert-Amyl methyl ether EPA 8260B 10 ND " <br /> 1,2-Dibromoethane EPA 8260B 10 ND " <br /> 1,2-Dschloroethane EPA 8260E 10 ND " <br /> Surrogate Dibromofluoromethane 50-150 102 % <br /> Surrogate l-2'Drchloroethaned4 50=150 104 " <br /> MW9 - - MJK0692-08 - - - Water - <br /> tert-Butyl alcohol OL05015 12/5/00 12/5/00 EPA 8260B 250 ND ug/l <br /> - >- Methyl tent-butyl ether - — -" -�--- " - " T EPA 8260B T 10 -- ND - <br /> Di-isopropyl ether EPA 8260B 10 ND " <br /> Ethyl tert-butyl ether EPA 8260B 10 ND " <br /> tert-Amyl methyl ether toEPA 8260B 10 ND " <br /> 1,2-Dibromoethane EPA 8260B 10 ND " <br /> 1,2-Dichloroethane toEPA 8260B 10 ND " <br /> Surrogate Dibromofluoromethane 50-150 104 % <br /> Surrogate 12-Dichloroethane-d4 50-150 104 11 <br /> MW 11 MJK0692-09 Water <br /> tert-Butyl alcohol OL05015 12/5/00 12/5/00 EPA 8260B 50 ND ug/l <br /> Methyl Cert-butyl ether " 11EPA 8260E 2 0 73 " <br /> Di-isopropyl ether EPA 8260B 20 ND " <br /> Ethyl tert-butyl ether EPA 8260B 20 ND " <br /> tert-Amyl methyl ether EPA 8260B 20 ND " <br /> 1,2-DEbromoethane EPA 8260B 2 0 ND " <br /> 1,2-Dichloroethane _ EPA 8260B 2 0 ND " <br /> Surrogate Dibromofluoromethane 50-150 100 % <br /> Surrogate 1,2-Drchloroethane-d4 50-150 126 S-030 <br /> Page 7 of 16 <br />