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Sequoia 885 Jarvis Drive <br /> 1` Morgan HEiI CA 95037 <br /> (408)776-9600 <br /> �,,,�► Analytical FAX 782-6308 <br /> www seqequouoialabs wm <br /> Blaine Tech Services(Shell) Project 440 W Charter Way <br /> 1680 Rogers Avenue Project Number 440 W Charter Way Reported <br /> San Jose CA,95112 Project Manager Nick Sudano 12/19/00 17 44 <br /> Volatile Organic Oxygenated Compounds by EPA Method 8260B - Quality Control <br /> Sequoia Analytical- San Carlos <br /> Reporting Spike Source %REC RPD <br /> Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch 0120001 -EPA 5030B PIT <br /> Matrix Spike Dnp(0120001-MSDI) Source L011219-03 Prepared&Analyzed 12/01/00 <br /> Methyl tert-butyl ether 453 200 ug/1 500 ND 906 600-140 360 250 <br /> Surrogate 1 2-Dichloroethane-d4 483 500 966 760-114 <br /> Batch 0120015-EPA 5030B PIT <br /> Blank(0120015-BLKI) Prepared&Analyzed 12/04/00 <br /> Ethanol ND 1000 ug/I <br /> Tert-butyl alcohol ND 100 " <br /> Methyl tert-butyl ether ND 200 " <br /> Di-isopropyl ether ND 200 " <br /> Ethyl tert-butyl ether ND 200 " <br /> AIWILamyl methyl ether ND 200 " <br /> ogate 11-Dichloroethane d4 461 500 912 760-114 <br /> Blank(0120015-BLK2) Prepared&Analyzed 12/05/00 <br /> 1,2-Dichloroethane ND 200 ug/I <br /> 1,2-13ibromoethane ND 200 " <br /> Ethanol ND 1000 " <br /> Tert-butyl alcohol ND 100 " <br /> Methyl tert-butyi ether ND 200 " <br /> Di-isopropyl ether ND 200 <br /> Ethyl tert-butyl ether ND 200 " <br /> Tert-amyl methyl ether ND 200 " <br /> Surrogate 12-Drchloroethane-d4 462 500 924 760-114 <br /> LCS(0120015-BSJ) Prepared&Analyzed 12/04/00 <br /> Methyl tert-butyl ether 439 200 ug/l 500 878 700-130 <br /> Surrogate 12-Dichloroethane-d4 471 500 944 760-114 <br /> oia Analytical-Morgan Hill The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document This analytical report must be reproduced in its entirety <br /> Page 12 of 14 <br />