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885 Jarvis Drive <br /> Sequoia Morgan Holl CA 95037 <br /> (408) 776-9600 <br /> Analytical FAX (408) 782-6308 <br /> 0 <br /> Blame Tech Services(Shell) Project Equrva Sampled 11/5/99 <br /> 1680 Rogers Avenue Project Number 440 W Charter Way Received 11/8/99 <br /> San Jose,CA 95112 Pro ect Manager Leah Davis Reported 11/22/99 <br /> W Total Purgeable Hydrocarbons (C6-C12),BTEX and MTBE by DHS LUFT/Quality Control <br /> Sequoia Analytical-Morgan Hill <br /> Date Spike Sample QC Reporting Limit Recov RPD RPD <br /> Analyte Analyzed Level Result Result Units Recov Limits % Limit % Notes* <br /> Batch 9110512 Date Prepared 11/16/99 Extraction Method EPA 5030E PIT <br /> Blank 9110512-BLK1 <br /> Purgeable Hydrocarbons 11/16/99 ND ug/l 500 <br /> Benzene ND 0 500 <br /> Toluene JVD 0 500 <br /> Ethylbenzene ND 0 500 <br /> Xylenes(total) ND 0 500 <br /> Methyl tert-butyl ether _ _ ND 2 50 <br /> Surrogate a a a-Trtfluorotoluene 100 9 52 700-130 952 <br /> LCS 9110512-BSI <br /> Benzene 11/16/99 100 9 08 ug/l 700-130 908 <br /> Toluene too 896 700-130 896 <br /> Ethylbenzene 100 890 700-130 890 <br /> Xylenes(total) _ __ _ _ W 3_0_0 _ 2_7_1 _ _ 700-130 903 <br /> IVogate a a a-Trrfluorotoluene 10 0 9 00 700-130 900 <br /> Matrix Spike 9110512-MS1 M9I1280-06 <br /> Benzene 11/16/99 10 0 ND 9 78 ug/l 600-140 978 <br /> Toluene l0 0 ND 9 74 600-140 974 <br /> Ethylbenzene 10 0 ND 9 83 600-140 983 <br /> Xylenes(total) _ _ 300 ND 294 _ 600-140 980 <br /> Surrogate a a a-Trrfluorotoluene 100 9 10 700-130 _91 0 <br /> Matrix Spike Dpp 9110512-MSDI M911280-06 <br /> Benzene 11/16/99 10 0 ND 9 75 ug/i 600-140 975 25 0 0 307 <br /> Toluene 10 0 ND 9 60 600-140 960 25 0 145 <br /> Ethylbenzene 10 0 ND 959 600-140 959 25 0 247 <br /> Xylenes(total) 300 ND 291 _ 600-140 970 250 103 <br /> Surrogate a a a-Trrfluorotoluene 100 9 01 700-130 901 <br /> Batch 9110513 Date Prepared 11/16/99 Extraction Method EPA 5030B IP/TI <br /> Blank 9110513-BLKI <br /> Purgeable Hydrocarbons 1 t/16/99 ND ug/1 500 <br /> Benzene ND 0 500 <br /> Toluene ND 0 500 <br /> Ethylbenzene ND 0 500 <br /> Xylenes(total) ND 0 500 <br /> Methyl tent-butyl ether _ ___ ND _ _ 250 <br /> Surrogate a a a-Trtflucrotoluene 100 103 700-130 103 <br /> Aft <br /> uoia Analytical-Morgan Hill *Refer to end ofreport for tett of notes and definitions <br /> Page 6 of 9 <br />