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COLUMBIA ANALYTICAL SERVICES,INC. <br /> Analytical Report <br /> Client. Equlva Services Service Request- 59901977 <br /> Protect SAP 121258/Incident 88870583 Date Collected- 6/29/99 <br /> Sample Matrix. Soil Date Received 6/30/99 <br /> TPH as Diesel <br /> Prep Method LOFT Units mg/Kg(ppm) <br /> Analysis Method California DHS LIFT Basis Wet <br /> Test Notes <br /> Dilution Date Date Result <br /> Sample Name Lab Code MRL Factor Extracted Analyzed Result Notes <br /> SP-10A 59901977-019 1 1 6/30/99 7/7/99 22 D4 <br /> SP-108 59901977-020 1 1 6/30199 7/8/99 49 D4 <br /> SP-IIA 59901977-021 1 1 6/30/99 7/7/99 5 D4 <br /> SP-118 59901977-022 1 1 6/30/99 7/8/99 18 D4 <br /> SP-12A 59901977-023 1 1 6/30/99 7/8/99 190 D4 <br /> SP-1213 59901977-024 1 1 6/30/99 7/8/99 13 D4 <br /> SP-13A 59901977-025 1 1 6/30/99 7/8199 13 <br /> SP-13B 59901977-026 1 1 6/30/99 718/99 10 <br /> SP-14A 59901977-027 1 1 6/30199 7/8/99 ND <br /> SP-14B 59901977-028 1 1 6/30/99 7/8/99 19 D5 <br /> SP-15A 59901977-029 1 1 6/30/99 718199 140 D4 <br />. SP-I5B 59901977-030 1 1 6/30/99 7/8/99 26 D4 <br /> SP-16A 59901977-031 1 1 6/30/99 7/8/99 110 D4 <br /> SP-16B 59901977-032 1 1 6/30/99 7/8/99 ND <br /> SP-17A 59901977-033 1 10 6/30/99 7/8/99 1300 <br /> SP-17B 59901977-034 1 1 6/30/99 7/8/99 7 <br /> SP-18A 59901977-035 1 1 6130/99 7/8/99 ND <br /> SP-18B 59901977-036 1 1 6/30/99 718199 6 <br /> D4 The sample contains a higher boiling point mixture of hydrocarbons and diesel quantitated as diesel <br /> D5 The sample contains a lower boiling point mixture of hydrocarbons and diesel quantitated as diesel <br /> Approved By Date J�7 <br /> IA/020597p <br /> Rl- .I <br />