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COLUMBIA ANALYTICAL SERVICES, INC. <br /> Analytical Report <br /> Client: Equiva Services Service Request 59901977 <br /> Project, SAP 121258/Incident 88870583 Date Collected 6/29/99 40 <br /> Sample Matrix. Soil Date Received. 6130/99 <br /> TPH as Gasoline <br /> Prep Method EPA 5030 Units mg/Kg(ppm) <br /> Analysis Method CA/LUFT Basis Wet <br /> Test Notes <br /> Dilution Date Date Result <br /> Sample Name Lab Code MRL Factor Extracted Analyzed Result Notes <br /> SP-1A 59901977-001 1 1 6130/99 7/3/99 ND <br /> SP-tB 59901977-002 1 1 6/30/99 713/99 ND <br /> SP-2A 59901977-003 1 1 6/30/99 7/3/99 ND <br /> SP-2B 59901977-004 I 1 6/30/99 714/99 ND <br /> SP-3A 59901977-005 1 1 6/30/99 713/99 ND <br /> SP-3B 59901977-006 1 1 6/30/99 714/99 ND <br /> SP-4A 59901977-007 1 1 6/30/99 7/4/99 ND <br /> SP-4B 59901977-008 1 1 6130/99 713/99 4 <br /> SP-5A 59901977-009 1 1 6/30/99 7/3/99 ND <br /> SP-5B 59901977-010 1 1 6130/99 7/3/99 ND <br /> SP-6A 59901977-011 1 1 6/30/99 7/3/99 ND <br /> SP-6B S9901977-012 1 1 6/30/99 713/99 ND <br /> SP-7A 59901977-013 1 1 6130/99 7/3/99 ND . <br /> SP-7B 59901977-014 1 1 6130/99 713/99 ND <br /> SP-8A 59901977-015 1 1 ' 6130/99 7/3/99 ND <br /> SP-8B 59901977-016 1 1 6130/99 7/3/99 ND <br /> SP-9A 59901977-017 1 1 6/30199 7/3/99 ND <br /> SP-9B 59901977-018 1 l 6130/99 7/3/99 ND <br /> Method Blank S990630-SBI 1 1 6/30/99 6130/99 ND <br /> Method Blank 5990630-SB2 1 1 6/30199 6,30/99 ND— <br /> Approved By Date <br /> IA/020$97p • <br /> Page 9 <br />