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COLUMBIA ANALYTICAL SERVICES,INC <br /> QA/QC Report <br /> . Client Egtllva Senu.es Service Request S990I977 <br /> Protect SAP 121259/1midtnt 88870583 Date.Analyzed 7/4/99 <br /> Initial Calibration Verification(ICV) Summary <br /> TPH as Gasoline <br /> Sample Namt ICV Units mg/Kg(ppm) <br /> Lab Code ICV I Basis Wet <br /> Test Notes <br /> ICV Source <br /> Prep Analysis True Percent Result <br /> Analvte Mo-thod Method Value Result Recovery Notes <br /> TPH as Gasoline EPA 5030 CA/LUFF 25 25 100 <br />• <br /> Approved By Date _VC7 <br /> ICV/032196 <br /> Page 16 <br />