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COLUMBIA ANALYTICAL SERVICES,INC <br /> Analytical Report <br /> Client Ecluiva Stxvlees So-rvice Request 19901977 <br /> Protect SAP 121258/Incident 88870583 Date Collee.ted 6/29/99 <br /> Sample Matrix Sud Date Received 6/30199 <br /> BTEX and TPH as Gasoline <br /> Sample Name SP-7AB COMP Units mg/Kg(ppm) <br /> Lab Code 59901977-043 Basis Wet <br /> -fest Notes <br /> Prep Analysis Dilution Date Date Result <br /> Analvte Method Method MRL Factor Extracted Analyzed Result Notes <br /> Methyl tert-Butyl Ethtr EPA 5030 8020 005 1 7/1/99 7/2/99 ND <br /> Benzene EPA 5030 8020 0 005 1 7/1/99 7/2/99 ND <br /> Toluene EPA 5030 8020 0 005 1 7/1199 7/2/99 ND <br /> Ethylbenzene EPA 5030 8020 0 005 1 7/1/99 7/2/99 ND <br /> Xylenes,Total EPA 5030 8020 0 005 1 7/1/99 712199 ND <br /> Approved By Date <br /> 1=0=97p <br /> Page 23 <br />