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COLUMBIA ANALYTICAL SERVICES,INC <br /> QA/QC Report <br /> Client Equi%a Servi"s Service Request 59901977 is <br /> Protect SAP 121258/lncldent 88870583 Date Analyzed 7/1/99 <br /> Initial Calibration Verification(ICV) Summary <br /> BTEX and TPH as Gasoline <br /> Sample Name 1CV Units mg/Kg(ppm) <br /> Lab Code 1CV1 Basis Wet <br /> Test Notes <br /> ICV Source <br /> Prep Analysis True Percent Result <br /> Anahte MLthud M4thod Value Result Recovery Notes <br /> TPH as Gasoline EPA 5030 CA/LUFt 25 25 100 <br /> Benzene EPA 5030 8020 2 5 25 100 <br /> Toluene EPA 5030 8020 2 5 25 100 <br /> Ethylbenzene EPA 5030 8020 2 5 2 5 100 <br /> Xvlenes Total EPA 5030 8020 75 7 3 97 <br /> Approved By Date "�r5s <br /> ICV/032196 �• <br /> Rwc 19 <br />