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COLUMBIA ANALYTICAL SERVICES,INC <br /> Analytical Report <br /> Client Equiva Services Service Request. K9904880 <br /> Protect Incident# 88870583/SAP#121258 Date Collected: 6/29/99 <br /> Sample Matrix Soil Date Received 6/30199 <br /> Date TCLP Performed 7/27/99 <br /> Date Extracted 7/28/99 <br /> Date Analyzed: 8/2199 <br /> Toxicity Characteristic Leaching Procedure(TCLP) <br /> EPA Method 1311 <br /> Metals <br /> Sample Name SP-I IAB COMP Units mgiL(ppm) <br /> Lab Code K9904880-047 Basis NA <br /> Test Notes <br /> Prep Analysis Dilution Regulatory Result <br /> Analyte Method Method MRL Factor Limit* Result Notes <br /> Lead EPA 3010 6010B 005 1 5 ND <br /> i <br /> * From 40 CFR Part 261 et al,and Federal Register,March 29, 1990 and June 29, 1990 <br /> Approved By Date OF- <br /> IS"052595 <br /> Page 4 <br />