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BC ANALYTICAL isORDER QC REPORT FOR G9602665 REPORTED 03/12/96 Page 1 MATRIX QC ACCURACY (SPIKES) BATCH QC REPORT SAMPLE DATE BATCH MS MSD TRUE PARAMETER NUMBER ANALYZED NUMBER % % RESULT UNIT 1. GRO 9602665*6 Benzene 03.05.96 96427 108 109 15.2 ug/L Toluene 03.05.96 96427 77 79 97.4 ug/L Ethylbenzene 03.05.96 96427 78 80 20.4 ug/L Total Xylene Isomers 03.05.96 96427 74 76 119 ug/L TPH (Gasoline Range) 03.05.96 96427 101 97 1100 ug/L a,a,a-Trifluorotoluene Rep. 03.05.96 96427 106 103 50.0 ug/L a,a,a--Trifluorotoluene Th. 03.05.96 96427 100 100 50.0 ug/L ?. Halocarbons 9602665*15 1, 1-Qichloroethene 03.06.96 963034 85 108 50.0 ug/L Chlorobenzene 03.06.96 963034 114 133 50.0 ug/L Trichloroethene 03.06.96 963034 108 131 50 0 ug/L Bromochloromethane Reported 03.06.96 963034 119 117 50 0 ug/L Bromochloromethane Theoretical 03.06.96 963034 100 100 50 0 ug/L 3. Halocarbons 9603100*6 1,1-Dlchloroethene 03.07.96 963035 77 92 50 0 ug/L Chlorobenzene 03.07.96 963035 105 119 50.0 ug/L Trichloroethene 03.07.96 963035 102 112 50.0 ug/L Wmochloromethane Reported 03.07.96 963035 113 113 50 0 ugh mochloromethane Theoretical 03.07.96 963035 100 100 50.0 ug/L 1 GRO 9602663*2 Benzene 03.07.96 96623 110 113 17.4 ug/L Toluene 03.07.96 96623 94 94 98.2 ug/L Ethylbenzene 03.07.96 96623 94 97 20 4 ug/L Total Xylene Isomers 03.07.96 96623 90 91 120 ug/L TPH (Gasoline Range) 03.07-96 96623 97 95 1100 ug/L a,a,a-Trifluorotoluene Rep. 03.07.96 96623 108 109 50 0 ug/L a,a,a-Trifluorotoluene Th. 03.07.96 96623 100 100 50.0 ug/L �. GRO 9603104*2 Benzene 03.05.96 96536 91 97 15.2 ug/L Toluene 03.05-96 96536 87 92 97.4 ug/L Ethylbenzene 03.05-96 96536 85 90 20.4 ug/L Total Xylene Isomers 03.05.96 96536 87 92 119 ug/L TPN (Gasoline Range) 03.05.96 96536 90 95 1100 ug/L a,a,a-Trifluorotoluene Rep 03.05.96 96536 105 108 50.0 ug/L a,a,a-Trifluorotoluene Th. 03.05.96 96536 100 100 50.0 ug/L